Other — Microwave discharge for rapid introduction of bimetallic-synergistic configuration to conductive catecholate toward long-term supercapacitor

Measurement evidence

Other

Microwave discharge for rapid introduction of bimetallic-synergistic configuration to conductive catecholate toward long-term supercapacitor · Jiang H., Xian J., Hu R. et al. · Chemical Engineering Journal · 2023 · 140804

1 measurement group · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Real-time infrared temperature monitoring, EDS and ICP elemental analysis across microwave pulse number

Elemental microanalysis and mapping Bulk elemental and compositional analysis

Zn,Ni-CAT-T4 · Electrode

Microwave pulses at 2450 MHz and 900 W; T1-T4 correspond to 1-4 pulses of 5 s each.

Atmosphere: Ar
Geometry: Ni-CAT at bottom of quartz reactor with Zn wire 20 mm above
Context: Pulse-series tuning of mixed-metal Zn content in conductive MOF.
Measurement source: 5-6 · 3.3. Optimization of bimetallic MOFs by microwave · Figure 4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Single-pulse peak temperature rise	649.2 C within 4 s	—	—	Text Exact Reported	5 · 3.3. Optimization of bimetallic MOFs by microwave · Figure 4a
Temperature drop after pulse suspension	drop 250 C within 1 s	—	—	Text Rounded Reported	5 · 3.3. Optimization of bimetallic MOFs by microwave · Figure 4a
Zn/Ni atomic ratio by EDS for Zn,Ni-CAT-T1	3.53 %	—	—	Text Exact Reported	6 · 3.3. Optimization of bimetallic MOFs by microwave · Figure 4b
Zn/Ni atomic ratio by EDS for Zn,Ni-CAT-T2	10.05 %	—	—	Text Exact Reported	6 · 3.3. Optimization of bimetallic MOFs by microwave · Figure 4b
Zn/Ni atomic ratio by EDS for Zn,Ni-CAT-T3	12.99 %	—	—	Text Exact Reported	6 · 3.3. Optimization of bimetallic MOFs by microwave · Figure 4b
Zn/Ni atomic ratio by EDS for Zn,Ni-CAT-T4Marked as a best value within this paper	14.53 %	—	—	Text Exact Reported	6 · 3.3. Optimization of bimetallic MOFs by microwave · Figure 4b
Zn/Ni atomic ratio by ICP for Zn,Ni-CAT-T4Marked as a best value within this paper	16.53 %	—	standard deviations all less than 0.21 % for four groups	Text Exact Reported	6 · 3.3. Optimization of bimetallic MOFs by microwave · Tables S1 and S2