Thermogravimetric analysis (TGA), Perkin-Elmer TGA-7
As-synthesised bulk NNU-27 · Powder
Heating rate 10 oC min-1 from room temperature to 800 oC; SI text says under atmosphere but does not specify gas.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| calculated DEF loss | 22.58% | — | — | Text Exact Reported | p003 · Thermal analysis · Figure S3 |
| TGA DEF loss below 400 oC | 22.12% below 400 oC | — | — | Text Exact Reported | p003 · Thermal analysis · Figure S3 |
| TGA ligand decomposition loss | 65.02% from 400 to 740 oC | — | — | Text Exact Reported | p003 · Thermal analysis · Figure S3 |