Microscopy Morphology — Anisotropic Redox Conductivity within a Metal-Organic Framework Material

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

EPD NU-1000 thin film on ZnO-coated FTO · Electrode

Hitachi SU8030 SEM; samples coated with 9 nm OsO4.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
EPD crystallite length	3.0 um annotation in Figure S3B	—	—	Visual Estimate Approximate	5 · Figure S3 · Figure S3B
EPD top-view crystallite orientation	Almost none of the crystallites are standing vertical to the electrode surface.	—	—	Caption Qualitative	11 · Figure S9 caption · Figure S9
EPD film thickness	0.8 um annotation in Figure S3B	—	—	Visual Estimate Approximate	5 · Figure S3 · Figure S3B

Solvothermal NU-1000 thin film on ZnO-coated FTO · Electrode

Hitachi SU8030 SEM; samples coated with 9 nm OsO4.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Solvothermal top-view crystallite orientation	Majority of crystallites standing vertical; several tilted or slanting; no horizontal rods detected with respect to electrode surface.	—	—	Caption Qualitative	11 · Figure S9 caption · Figure S9
Solvothermal film/crystallite height	2.7 um annotation in Figure S3A	—	—	Visual Estimate Approximate	5 · Figure S3 · Figure S3A