Porosity — A semiconducting layered metal-organic framework magnet

Measurement evidence

Porosity

A semiconducting layered metal-organic framework magnet · Yang C., Dong R., Wang M. et al. · Nature Communications · 2019 · 3260

2 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 sorption/BET and DFT pore-size analysis

as-synthesised K3Fe2[PcFe-O8] dark black powder · Powder

Low-pressure N2 sorption at 77 K after supercritical CO2 drying and 80 C overnight activation.

Temperature
77
Atmosphere
nitrogen sorption
Geometry
powder
Context
pristine target MOF
Measurement source
p002 · Synthesis and structural analysis · Supplementary Figure 7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface areaMarked as a best value within this paper206 m2 g-1Text
Rounded Reported
p002 · Synthesis and structural analysis · Supplementary Figure 7
average microporous pore sizeMarked as a best value within this paper~1.4 nm~Caption
Approximate
p014 · Supplementary Figure 7 · Supplementary Figure 7

N2 sorption/BET and DFT pore-size analysis

LixFe2[PcFe-O8] powder · Powder

N2 adsorption isotherm at 77 K after supercritical CO2 drying.

Temperature
77
Atmosphere
nitrogen sorption
Geometry
powder
Context
Li-counterion analogue
Measurement source
p014 · Supplementary Figure 7 · Supplementary Figure 7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface areaMarked as a best value within this paper343 m2 g-1Caption
Rounded Reported
p014 · Supplementary Figure 7 · Supplementary Figure 7
average microporous pore sizeMarked as a best value within this paper~1.45 nm~Caption
Approximate
p014 · Supplementary Figure 7 · Supplementary Figure 7