Diffraction Structure — Conductive metal–organic framework with redox metal center as cathode for high rate performance lithium ion battery

Measurement evidence

Diffraction Structure

Conductive metal–organic framework with redox metal center as cathode for high rate performance lithium ion battery · Gu S., Bai Z., Majumder S. et al. · Journal of Power Sources · 2019 · 22-29

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XRD before and after 150 degC heating

X-ray diffraction and scattering

Heat-treated Cu3(HHTP)2 powder · Powder

Cu3(HHTP)2 powder compared before and after heating at 150 degC to remove DMF.

Context: pristine MOF powder before/after activation heating
Measurement source: 2 · Supplementary figures and tables · Fig. S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
crystalline structure after 150 degC heating	no change in crystalline structure after heating treatment	—	—	Text Qualitative	3 · 3.1. Structure and morphology · Fig. S1

PXRD with Rigaku Smartlab 9 kW, Cu Kalpha radiation

X-ray diffraction and scattering

Cu3(HHTP)2 crystalline powder · Powder

2theta range 3-40 deg; experimental pattern compared with slipped-parallel and eclipsed simulated stacking models.

Context: pristine MOF powder
Measurement source: 2 · 2.3. Characterizations · Fig. 1b

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Cu...Cu interlayer distance	about 4.25 Angstrom	0.425 nm	—	Caption Approximate	2 · Figure caption · Fig. 1a
hexagonal pore/open-window size	about 1.82 nm	—	—	Caption Approximate	2 · Figure caption · Fig. 1a
main XRD diffraction peak positions	2theta = 4.7, 9.5, 12.6 and 16.5 deg	—	—	Text Rounded Reported	3 · 3.1. Structure and morphology · Fig. 1b
stacking model assignment	slipped-parallel stacking; measured peak about 2theta = 27.5 deg corresponds to (002)	—	—	Text Approximate	3 · 3.1. Structure and morphology · Fig. 1b