Microscopy Morphology — Nanoporous synthetic metal: A nickel MOF with an amino-functionalized macrocyclic ligand

Measurement evidence

Microscopy Morphology

Nanoporous synthetic metal: A nickel MOF with an amino-functionalized macrocyclic ligand · Pham H.T.B., Fang X., Choi J.Y. et al. · Chem · 2025 · 102487

4 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM and HRTEM

Cu-HATC powders · Powder

SEM and HRTEM of Cu-HATC; lattice distance in inset

Context
pristine Cu-HATC
Measurement source
S33 · Synthesis and characterization of Cu-HATC · Figure S41
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
lattice distance2.22 nmCaption
Exact Reported
S33 · Synthesis and characterization of Cu-HATC · Figure S41

HRTEM

Ni-HATC bulk powders · Powder

High-resolution TEM; lattice distance along [001] direction

Context
pristine Ni-HATC
Measurement source
p. 3 · Synthesis and characterization of Ni-HATC · Figure 2E
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
lattice distance2.26 nmText
Exact Reported
p. 3 · Synthesis and characterization of Ni-HATC · Figure 2E

scanning electron microscopy (SEM)

Ni-HATC thin film on glass · Thin Film

Ni-HATC thin film imaged at multiple magnifications

Geometry
thin film on glass
Context
pristine Ni-HATC thin film
Measurement source
25 · Figure S31 · S31
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
thin-film morphologySEM revealed homogeneous thin film with particle morphology resembling bulk powders.Text
Qualitative
4 · Thin-film characterisation

surface profilometry

Ni-HATC thin film on glass · Thin Film

Thin-film thickness measured on a glass slide using Bruker DektakXTA surface profilometer.

Geometry
thin film on glass
Context
pristine Ni-HATC
Measurement source
p. 4 · Synthesis and characterization of Ni-HATC · Figure S28
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
thin-film thicknessapproximately 100 nmText
Approximate
p. 4 · Synthesis and characterization of Ni-HATC · Figure S28