Diffraction Structure — Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid

3 measurement groups · 19 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

ELT@Z100 · Pellet

Measured in air; data analysed by Le Bail method in TOPAS.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
ELT@Z100 cubic lattice parameter a	17.04(1) A	—	—	Visual Estimate Rounded Reported	S3 · Supporting Information · Figure S3
ELT@Z100 crystallite diameter from Le Bail fit	10.9(2) nm	—	—	Visual Estimate Rounded Reported	S3 · Supporting Information · Figure S3
ELT@Z100 Le Bail Rwp factor	19.4%	—	—	Visual Estimate Rounded Reported	S3 · Supporting Information · Figure S3
ELT@Z100 Le Bail goodness-of-fit S	1.37	—	—	Visual Estimate Rounded Reported	S3 · Supporting Information · Figure S3
ELT@Z100 cubic unit-cell volume V	4950(9) A^3	—	—	Visual Estimate Rounded Reported	S3 · Supporting Information · Figure S3
Crystallite diameter from Le Bail profile fitting	about 10 nm	—	—	Text Approximate	3 · Results and Discussion · Figure 3
ZIF-8 structure retained after lithium-doped IL loading	ZIF-8 crystal structure was maintained after mixing with (EMI0.8Li0.2)TFSA and heating	—	—	Text Qualitative	3 · Results and Discussion · Figure 3
XRPD evidence for guest incorporation	relative intensity of 011 decreased and 013 increased after incorporation	—	—	Text Qualitative	3 · Results and Discussion · Figure 3

ELT@Z75 · Pellet

Measured in air; data analysed by Le Bail method in TOPAS.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
ELT@Z75 cubic lattice parameter a	17.012(9) A	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S2
ELT@Z75 crystallite diameter from Le Bail fit	12.9(2) nm	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S2
ELT@Z75 Le Bail Rwp factor	19.4%	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S2
ELT@Z75 Le Bail goodness-of-fit S	1.37	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S2
ELT@Z75 cubic unit-cell volume V	4923(8) A^3	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S2

ZIF-8 nanoparticles · Powder

Measured in air; data analysed by Le Bail method in TOPAS.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
ZIF-8 nanoparticles cubic lattice parameter a	16.96(1) A	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S1
ZIF-8 nanoparticles crystallite diameter from Le Bail fit	8.47(9) nm	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S1
ZIF-8 nanoparticles Le Bail Rwp factor	16.4%	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S1
ZIF-8 nanoparticles Le Bail goodness-of-fit S	1.37	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S1
ZIF-8 nanoparticles cubic unit-cell volume V	4877(10) A^3	—	—	Visual Estimate Rounded Reported	S2 · Supporting Information · Figure S1
Synthesised ZIF-8 diffraction character	very broad and weak diffraction because of small crystal sizes	—	—	Text Qualitative	3 · Results and Discussion · Figure 3