Microscopy Morphology — From insulator to semiconductor: effect of host-guest interactions on charge transport in M-MOF-74 metal-organic frameworks

Measurement evidence

Microscopy Morphology

From insulator to semiconductor: effect of host-guest interactions on charge transport in M-MOF-74 metal-organic frameworks · Angel S.M., Barnett N.S., Talin A.A. et al. · Journal of Materials Chemistry C · 2024 · 2699-2704

1 measurement group · 1 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Scanning electron microscopy (SEM)

TCNQ@Cu-MOF-74 pellet · Pellet

JEOL JSM-7600F thermal field emission SEM; samples sputter-coated with gold; 10 kV acceleration voltage, 2000x magnification, 8.0 mm working distance.

Geometry
Solid MOF particles; main Fig. 1 and SI Fig. S3.
Context
Parent, TCNQ-loaded, and H4TCNQ-loaded M-MOF-74 controls.
Measurement source
S-5-S-7 · Characterization methods; SEM Images · Fig. S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Morphology after TCNQ infiltrationMOFs retained rough, porous morphology with some polycrystallinity; SEM showed no metal-containing TCNQ nanowires.Text
Qualitative
2700 · Results and discussion · Fig. 1b-e