Spectroscopy — Nanoporous gold induced vertically standing 2D NiCo bimetal-organic framework nanosheets for non-enzymatic glucose biosensing

Measurement evidence

Spectroscopy

Nanoporous gold induced vertically standing 2D NiCo bimetal-organic framework nanosheets for non-enzymatic glucose biosensing · Li W., Lv S., Wang Y. et al. · Sensors and Actuators, B: Chemical · 2019 · 652-658

3 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XPS Co 2p

Co-MOFNs control · Unknown

High-resolution XPS Co 2p of Co-MOFNs and NiCo-MOFNs

Geometry
ESCALAB-250, Al Kalpha
Context
target and Co control
Measurement source
655 · 3.3 Characterization · Fig. 4c-d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co-MOFNs Co 2p1/2 binding energy796.8 eVText
Rounded Reported
655 · 3.3 Characterization · Fig. 4c
Co-MOFNs Co 2p3/2 binding energy781.1 eVText
Rounded Reported
655 · 3.3 Characterization · Fig. 4c
NiCo-MOFNs Co 2p shiftMarked as a best value within this paperCo 2p peaks shift toward higher energyText
Qualitative
655 · 3.3 Characterization · Fig. 4d

XPS N 1s

vertical NiCo(1:1)-MOFNs array on nanoporous gold, 4 h growth · Electrode

High-resolution XPS N 1s compared with Ni-MOFNs and Co-MOFNs

Geometry
ESCALAB-250, Al Kalpha
Context
target and pristine controls
Measurement source
655 · 3.3 Characterization · Fig. 4a-b, Fig. S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-MOFNs N 1s N-H binding energy399.8 eVText
Rounded Reported
655 · 3.3 Characterization · Fig. 4a
NiCo-MOFNs N-H N 1s binding energy399.6 eVText
Rounded Reported
655 · 3.3 Characterization · Fig. 4b
NiCo-MOFNs metal nitride N 1s binding energyMarked as a best value within this paper398.9 eVText
Rounded Reported
655 · 3.3 Characterization · Fig. 4b

XPS Ni 2p

Ni-MOFNs control · Unknown

High-resolution XPS Ni 2p of Ni-MOFNs and NiCo-MOFNs

Geometry
ESCALAB-250, Al Kalpha
Context
target and Ni control
Measurement source
655 · 3.3 Characterization · Fig. 4e-f
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-MOFNs Ni 2p1/2 binding energy874.6 eVText
Rounded Reported
655 · 3.3 Characterization · Fig. 4e
Ni-MOFNs Ni 2p3/2 binding energy856.65 eVText
Exact Reported
655 · 3.3 Characterization · Fig. 4e
NiCo-MOFNs Ni 2p shiftMarked as a best value within this paperNi 2p peaks shifted to lower energy compared to Ni-MOFNsText
Qualitative
655 · 3.3 Characterization · Fig. 4f