Thermogravimetric analysis
As-synthesised bulk compound 1 · Powder
Perkin-Elmer Pyris Diamond TG/DTA, 30-800 deg C under nitrogen atmosphere.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA measurement range | 30-800 deg C under nitrogen | — | — | Text Range | p002 · 2.1 Physical measurements · Fig. S3 |
| first major TGA mass-loss onset/step region | approximately 150-180 deg C first major drop | — | visual estimate from rendered TGA axis | Figure Axis Range | S3 · Supporting Information · Figure S3 |
| residual mass at 800 deg C | approximately 22% weight remaining at 800 deg C | — | visual estimate from rendered TGA axis | Figure Axis Approximate | S3 · Supporting Information · Figure S3 |
| second major TGA mass-loss step region | approximately 390-450 deg C second major drop | — | visual estimate from rendered TGA axis | Figure Axis Range | S3 · Supporting Information · Figure S3 |