Elemental analysis and KBr FT-IR spectroscopy
As-synthesised bulk compound 1 · Powder
Elemental analysis on Perkin-Elmer 240C; IR in KBr over 4500-500 cm^-1 using Shimadzu FT-IR spectrum RX1.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| empirical formula from elemental analysis | C14H14Cl2CoN2O6 (436.10) | — | — | Text Exact Reported | p002 · 2.2.1 Preparation |
| FT-IR asymmetric carboxylate stretch | 1611 cm^-1 | — | — | Text Exact Reported | p002 · 2.2.1 Preparation |
| FT-IR symmetric carboxylate stretch | 1347 cm^-1 | — | — | Text Exact Reported | p002 · 2.2.1 Preparation |
| isolated yield | 0.06 g (68.8%) | — | — | Text Exact Reported | p002 · 2.2.1 Preparation |