cMOF Evidence Base
Other — High-resolution structure of Zn3(HOTP)2 (HOTP = hexaoxidotriphenylene), a three-dimensional conductive MOF

Measurement evidence

Other

High-resolution structure of Zn3(HOTP)2 (HOTP = hexaoxidotriphenylene), a three-dimensional conductive MOF · Zhang K.J., Chen T., Oppenheim J.J. et al. · Chemical Science · 2025 · 12416-12420

2 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Isolated yield and elemental analysis

Bulk elemental and compositional analysis

As-synthesised Zn3(HOTP)2 black/dark-blue crystalline powder · Powder

Yield after solvothermal synthesis and washing; elemental analysis by Robertson Microlit Laboratories.

Context
pristine Zn3(HOTP)2
Measurement source
p004 · 2. Synthetic Procedures
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Measured elemental carbonC: 43.27%——Text
Exact Reported		p004 · 2. Synthetic Procedures
Measured elemental hydrogenH: 3.36%——Text
Exact Reported		p004 · 2. Synthetic Procedures
Measured elemental nitrogenN: 0.87%——Text
Exact Reported		p004 · 2. Synthetic Procedures
Recovered product mass8.92 mg——Text
Exact Reported		p004 · 2. Synthetic Procedures
Isolated yield35% yield——Text
Exact Reported		p004 · 2. Synthetic Procedures

Thermogravimetric analysis (TGA)

Thermogravimetric analysis

As-synthesised Zn3(HOTP)2 black/dark-blue crystalline powder · Powder

TA Instruments Q500; 2.0 deg C/min under dry air gas flow of 5 mL/min on platinum pan from room temperature to 600 deg C.

Atmosphere
dry air
Geometry
platinum pan
Context
as-synthesised pristine Zn3(HOTP)2
Measurement source
p003 · Methods; Thermogravimetric analysis · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Gradual framework decomposition upper temperature~500 deg C—~150-500 deg CCaption
Range		p007 · 5. Thermogravimetric analysis (TGA) · Figure S3
Gradual framework decomposition onset~150 deg C—~150-500 deg CCaption
Range		p007 · 5. Thermogravimetric analysis (TGA) · Figure S3
Initial TGA mass loss upper bound below 150 deg C~7-10%—~7-10%Caption
Range		p007 · 5. Thermogravimetric analysis (TGA) · Figure S3
Initial TGA mass loss lower bound below 150 deg C~7-10%—~7-10%Caption
Range		p007 · 5. Thermogravimetric analysis (TGA) · Figure S3