Diffraction Structure — Two-Dimensional Conjugated Metal-Organic Frameworks with Large Pore Apertures and High Surface Areas for NO2 Selective Chemiresistive Sensing

Measurement evidence

Diffraction Structure

Two-Dimensional Conjugated Metal-Organic Frameworks with Large Pore Apertures and High Surface Areas for NO2 Selective Chemiresistive Sensing · Chen P., Su X., Wang C. et al. · Angewandte Chemie - International Edition · 2023 · e202306224

1 measurement group · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD with Pawley refinement; simulated AA/AB stacking models

X-ray diffraction and scattering

HIOTP-Ni black powder · Powder

Powder X-ray diffraction; Materials Studio/Reflex simulations compared with experimental patterns.

Context: pristine HIOTP-M powders
Measurement source: p002-p003 · Crystalline structures · Figure 2c-d / Figure S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
HIOTP-Cu a/b lattice parameter	a = b = 38.17 Angstrom	—	—	Text Exact Reported	p002 · Crystalline structures · Figure S6
HIOTP-Cu c lattice parameter	c = 3.34 Angstrom	—	—	Text Exact Reported	p002 · Crystalline structures · Figure S6
HIOTP-Cu Pawley Rwp	Rwp = 3.11%	—	—	Text Exact Reported	p002 · Crystalline structures · Figure S6
HIOTP-Ni a/b lattice parameter	a = b = 37.90 Angstrom	—	—	Text Exact Reported	p002 · Crystalline structures · Figure 2d
HIOTP-Ni c lattice parameter	c = 3.28 Angstrom	—	—	Text Exact Reported	p002 · Crystalline structures · Figure 2d
HIOTP-M principal PXRD peaks	2.70, 4.65, 5.40 and 27.20 deg assigned to (100), (110), (200), and (001)	—	—	Text Rounded Reported	p002 · Crystalline structures · Figure 2c
HIOTP-Ni Pawley Rwp	Rwp = 1.97%	—	—	Text Exact Reported	p002 · Crystalline structures · Figure 2d