Grazing-incidence X-ray diffraction and scanning electron microscopy
Pristine Cu3(BTC)2 thin-film device on quartz · Thin Film
Cu3(BTC)2 thin films before/after TCNQ infiltration; supporting XRD plotted for HKUST-1 before and after infiltration.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu3(BTC)2 nominal film thickness | 200 nm nominal thickness | — | — | Text Rounded Reported | main p.6, article p.3458 · Experimental Section |
| Grain size range | tens of nanometers to about 1 um depending on film thickness and exact growth conditions | — | — | Text Range | main p.2, article p.3454 · Results · Figure 1a |
| Preferred orientation | polycrystalline with preferred orientation along the (111) direction | — | — | Text Qualitative | main p.6, article p.3458 · Experimental Section · Figure S1 |