Other — A new semiconducting coordination polymer consisting of copper(I)-iodide and 3-pyridinecarboxaldehyde

Measurement evidence

Other

A new semiconducting coordination polymer consisting of copper(I)-iodide and 3-pyridinecarboxaldehyde · Himoto K., Horii T., Syoji T. et al. · Inorganic Chemistry Communications · 2018 · 34-37

2 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Elemental analysis of isolated product

Bulk elemental and compositional analysis

Powdered sample of [CuI(3-Py-CHO)]n · Powder

Calculated and found C/H/N values reported for C6H5ICuNO.

Geometry: Bulk crystalline product/powder
Context: pristine_framework
Measurement source: 1.2. Synthesis

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Calculated carbon content	C, 24.22	—	—	Text Exact Reported	1.2. Synthesis
Calculated hydrogen content	H, 1.69	—	—	Text Exact Reported	1.2. Synthesis
Calculated nitrogen content	N, 4.71	—	—	Text Exact Reported	1.2. Synthesis
Found carbon content	C, 24.17	—	—	Text Exact Reported	1.2. Synthesis
Found hydrogen content	H, 1.73	—	—	Text Exact Reported	1.2. Synthesis
Found nitrogen content	N, 4.77	—	—	Text Exact Reported	1.2. Synthesis
Isolated product mass	0.73 g	—	—	Text Exact Reported	1.2. Synthesis
Isolated yield	49%	—	—	Text Exact Reported	1.2. Synthesis

Thermogravimetric and differential thermal analysis

Calorimetry and thermal analysis Thermogravimetric analysis

Powdered sample of [CuI(3-Py-CHO)]n · Powder

TG-DTA carried out with a RIGAKU Thermo Plus 8120 under flowing N2 gas.

Atmosphere: flowing N2
Geometry: Powder sample
Context: pristine_framework
Measurement source: 1.4. Physical Measurements · Figure S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TG-DTA atmosphere	measured under N2 atmosphere	—	—	Caption Qualitative	SI p.S5 · Supporting figures · Figure S5
Approximate TG weight loss after decomposition	approximately 35% remaining mass after major loss near 460 K	—	—	Visual Estimate Uncertain	SI p.S5 · Rendered TG-DTA curve · Figure S5