Diffraction Structure — Metal-halide porous framework superlattices

9 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SC-XRD and PXRD

X-ray diffraction and scattering

CdI2@NU-600 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

SC-XRD and PXRD

X-ray diffraction and scattering

NiBr2@PCN-700 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

SC-XRD and PXRD

X-ray diffraction and scattering

PbBr2@PCN-606 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

SC-XRD and PXRD

X-ray diffraction and scattering

PbBr2@PCN-700 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

SC-XRD and PXRD

X-ray diffraction and scattering

PbI2@NU-1000 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PbI2 cluster size	4.3 x 4.5 x 7.4 A3	—	—	Text Rounded Reported	419 · Synthesis and X-ray crystal structures
PbI2 sublattice dimensionality	0D distorted cuboid PbI2 clusters	—	—	Text Exact Reported	419 · Synthesis and X-ray crystal structures

SC-XRD and PXRD

X-ray diffraction and scattering

PbI2@NU-600 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

SC-XRD and PXRD

X-ray diffraction and scattering

PbI2@PCN-606 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Pb2+ content final	29.4%	—	—	Text Rounded Reported	S4 · ICP-OES data
Pb2+ content start	7.1%	—	—	Text Rounded Reported	S4 · ICP-OES data
Pb2+/Zr4+ ratio final PbI2@PCN-606	~1.9	—	—	Text Approximate	S4 · ICP-OES data
PbI2 sublattice dimensionalityMarked as a best value within this paper	fully filled 2D PbI2@PCN-606	—	—	Caption Exact Reported	420 · Fig. 1 caption · Fig. 1h
monolayer thickness	approximately 7.2 A	—	—	Text Approximate	419 · Synthesis and X-ray crystal structures

SC-XRD and PXRD

X-ray diffraction and scattering

PbI2@PCN-609 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PbI2 sublattice dimensionality	half-filled 2D PbI2@PCN-609	—	—	Caption Exact Reported	420 · Fig. 1 caption · Fig. 1f

SC-XRD and PXRD

X-ray diffraction and scattering

PbI2@PCN-700 single crystals · Single Crystal

Single-crystal XRD for atomic structure; PXRD compared with simulated patterns

Temperature: 100-173
Geometry: single crystal/powder
Context: guest-loaded superlattice
Measurement source: 419-420 · Synthesis and X-ray crystal structures · Fig. 1 and Extended Data

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PbI2 sublattice dimensionality	1D chains/nanorods	—	—	Text Exact Reported	419 · Synthesis and X-ray crystal structures