Microscopy Morphology — Synthesis and characterization of Fe3O4-supported metal–organic framework MIL-101(Fe) for a highly selective and sensitive hydrogen peroxide electrochemical sensor

Measurement evidence

Microscopy Morphology

Synthesis and characterization of Fe3O4-supported metal–organic framework MIL-101(Fe) for a highly selective and sensitive hydrogen peroxide electrochemical sensor · Salman F., Zengin A., Celik Kazici H. · Ionics · 2020 · 5221-5232

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM and TEM

MIL-101(Fe)@Fe3O4 nanoparticles · Powder

SEM/TEM comparison after MIL-101(Fe) deposition

Context
MIL-101(Fe)@Fe3O4 composite powder
Measurement source
5223 · SEM and TEM analysis · Fig. 1b,d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Core-shell morphologydark Fe3O4 core and bright MIL-101(Fe) outer layerQualitative
Qualitative
5223 · SEM and TEM analysis · Fig. 1d
MIL-101(Fe) shell thicknessapproximately 25 nmText
Approximate
5223 · SEM and TEM analysis · Fig. 1d

SEM and TEM

Fe3O4 nanoparticles · Powder

SEM at 10 kV; TEM with FEI Tecnai G2 Spirit

Context
Fe3O4 component control
Measurement source
5222-5223 · Chemicals and materials; SEM and TEM analysis · Fig. 1a,c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Fe3O4 nanoparticle diameter~243 nmText
Approximate
5223 · SEM and TEM analysis · Fig. 1c