Microscopy Morphology — Redox-Active Ni(II) Nodes Induced Electrochromism in a Two-Dimensional Conductive Metal-Organic Framework

Measurement evidence

Microscopy Morphology

Redox-Active Ni(II) Nodes Induced Electrochromism in a Two-Dimensional Conductive Metal-Organic Framework · Pan L., Li R., Zhang C. et al. · ACS Applied Electronic Materials · 2022 · 2915-2922

2 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM and cross-section SEM

Ni3(HITP)2-362 nm/FTO electrode · Electrode

Field-emission SEM (Hitachi S-4800) used to inspect surface uniformity and cross-section thickness for the film series.

Geometry
FTO-supported thin films
Context
pristine Ni3(HITP)2 films on FTO
Measurement source
p002 · Results and Discussion · Figures S5-S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Film thickness, Ni3(HITP)2-205205 nmSI Table
Exact Reported
S-18 / p018 · Supporting Table S2 · Table S2
Film thickness, Ni3(HITP)2-290290 nmSI Table
Exact Reported
S-18 / p018 · Supporting Table S2 · Table S2
Film thickness, Ni3(HITP)2-362362 nmSI Table
Exact Reported
S-18 / p018 · Supporting Table S2 · Table S2
Film thickness, Ni3(HITP)2-435435 nmSI Table
Exact Reported
S-18 / p018 · Supporting Table S2 · Table S2
Film thickness, Ni3(HITP)2-524524 nmSI Table
Exact Reported
S-18 / p018 · Supporting Table S2 · Table S2

TEM/HRTEM and FFT

Ni3(HITP)2 precipitate/powder · Powder

HRTEM images obtained using a JEOL JEM-2100 at 50 kV; FFT image reported in SI.

Context
pristine Ni3(HITP)2 precipitate
Measurement source
p002 · Results and Discussion · Figure 1c and Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TEM pore diameteraround 2 nmText
Approximate
p002 · Results and Discussion · Figure 1c