Microscopy Morphology — Catalysis-Assisted Synthesis of Two-Dimensional Conductive Metal–Organic Framework Films with Controllable Orientation

3 measurement groups · 14 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

edge-on Cu3(HHTP)2 film from air-saturated precursor · Thin Film

air-saturated Cu3(HHTP)2 growth and edge-on orientation

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
air-saturated O2 concentration	~0.26 mM	—	—	Text Approximate	17062 · Results and Discussion · Figure 7; Figure S25
edge-on orientation assignment	2D layers perpendicular to substrate	—	—	Text Qualitative	17062 · Results and Discussion · Figure 7
edge-on growth rate in first 3 h	2.9 nm min-1	—	—	Text Exact Reported	17062 · Results and Discussion · Figure 7; Figure S25
edge-on growth rate after 5 h	1.2 nm min-1	—	—	Text Exact Reported	17062 · Results and Discussion · Figure 7; Figure S25
edge-on nanosheet thickness	~35 nm	—	—	Text Approximate	17062 · Results and Discussion · Figure 7; Figure S25

face-on Cu3(HHTP)2 growth-series films · Thin Film

O2-saturated Cu3(HHTP)2 growth from 1 min to 4 h

Context: pristine conductive MOF film
Measurement source: 17061-17062 · Results and Discussion · Figure 6; Figures S23-S24

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
4 h bottom layer thickness	~3500 nm	—	—	Text Approximate	17061-17062 · Results and Discussion · Figure 6; Figure S24
4 h top nanosheet lateral size	500 nm	—	—	Text Exact Reported	17061-17062 · Results and Discussion · Figure 6; Figure S24
4 h top nanosheet thickness	~42 nm	—	—	Text Approximate	17061-17062 · Results and Discussion · Figure 6; Figure S24
4 h top layer thickness	~540 nm	—	—	Text Approximate	17061-17062 · Results and Discussion · Figure 6; Figure S24
face-on Cu3(HHTP)2 thickness at 120 min	2460 nm	—	—	Text Exact Reported	17061-17062 · Results and Discussion · Figure 6; Figure S24
face-on Cu3(HHTP)2 thickness at 1 min	about 190 nm	—	—	Text Approximate	17061-17062 · Results and Discussion · Figure 6; Figure S24
face-on average growth rate first 5 min	103 nm min-1	—	—	Text Exact Reported	17061-17062 · Results and Discussion · Figure 6; Figure S24
face-on average growth rate after 30 min	13.7 nm min-1	—	—	Text Exact Reported	17061-17062 · Results and Discussion · Figure 6; Figure S24

patterned Cu3(HHTP)2 films on varied substrates · Thin Film

Patterned Cu3(HHTP)2 on glass, PDMS, cotton, parylene, PVC, nylon and other supports

Context: pristine conductive MOF film
Measurement source: 17061 · Results and Discussion · Figure 5; Figures S18-S22

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
patterned film feature sizes	micrometre to centimetre scale	—	—	Text Qualitative	17061 · Results and Discussion · Figure 5