Spectroscopy — Electrochemical immunoassay for the carcinoembryonic antigen based on Au NPs modified zeolitic imidazolate framework and ordered mesoporous carbon

Measurement evidence

Spectroscopy

Electrochemical immunoassay for the carcinoembryonic antigen based on Au NPs modified zeolitic imidazolate framework and ordered mesoporous carbon · Zhang Y., Zhang Z., Rong S. et al. · Microchimica Acta · 2020 · 264

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR and Raman spectroscopy

ZIF-8 powder · Powder

FTIR and Raman spectra of ZIF-8 nanoparticles in the Supporting Information.

Context
Pristine ZIF-8 chemical bonding.
Measurement source
SI rendered text · FTIR and Raman spectra of ZIF-8 · Fig. S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
FTIR C=N stretching band1585 cm-1Text
Exact Reported
SI rendered text · FTIR and Raman spectra of ZIF-8 · Fig. S1a
FTIR Zn-N stretching band419 cm-1Text
Exact Reported
SI rendered text · FTIR and Raman spectra of ZIF-8 · Fig. S1a
Raman Zn-N stretching band174 cm-1Text
Exact Reported
SI rendered text · FTIR and Raman spectra of ZIF-8 · Fig. S1b

X-ray photoelectron spectroscopy

Au@ZIF-8 nanoparticles · Powder

XPS survey and Au 4f, Zn 2p, N 1s and O 1s spectra of Au@ZIF-8.

Context
Au@ZIF-8 composite chemistry and Au valence.
Measurement source
4-5 · Material characterization · Fig. 3b-f
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Au 4f5/2 binding energy87.6 eVText
Exact Reported
4 · Material characterization · Fig. 3c
Au 4f7/2 binding energy84.1 eVText
Exact Reported
4 · Material characterization · Fig. 3c
N 1s binding energyabout 399 eVText
Approximate
4 · Material characterization · Fig. 3e
Zn 2p1/2 binding energy1044.8 eVText
Exact Reported
4 · Material characterization · Fig. 3d
Zn 2p3/2 binding energy1021.8 eVText
Exact Reported
4 · Material characterization · Fig. 3d