Spectroscopy — Facile one-pot synthesis of Co coordination polymer spheres doped macroporous carbon and its application for electrocatalytic oxidation of glucose

Measurement evidence

Spectroscopy

Facile one-pot synthesis of Co coordination polymer spheres doped macroporous carbon and its application for electrocatalytic oxidation of glucose · Meng T., Shang N., Zhao J. et al. · Journal of Colloid and Interface Science · 2021 · 135-146

2 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FT-IR spectroscopy

Infrared spectroscopy

Co CPSs/MPC-2 · Powder

FT-IR spectra of MPC, H2IPA, Co-CPSs and Co-CPSs/MPC-2.

Geometry: KBr plate
Context: pristine controls and composite
Measurement source: 137-138 · 3.1 · Fig. 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co CPSs C-O vibration peak	1078 cm^-1	—	—	Text Exact Reported	138 · 3.1 · Fig. 2
C=O stretching shift upon Co CPS formation	1696 to 1612 cm^-1	—	—	Text Exact Reported	138 · 3.1 · Fig. 2
Co CPSs phenyl vibration peak	711 cm^-1	—	—	Text Exact Reported	138 · 3.1 · Fig. 2
Co CPSs phenyl vibration peak	745 cm^-1	—	—	Text Exact Reported	138 · 3.1 · Fig. 2

X-ray photoelectron spectroscopy (XPS)

X-ray photoelectron spectroscopy

Co CPSs/MPC-2 · Powder

Survey and deconvoluted O 1s, C 1s and Co 2p spectra for Co CPSs/MPC-2.

Context: target composite
Measurement source: 138-139 · 3.1 · Fig. 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
C 1s C=C peak	284.7 eV	—	—	Text Exact Reported	139 · 3.1 · Fig. 3C
C 1s C-O peak	285.2 eV	—	—	Text Exact Reported	139 · 3.1 · Fig. 3C
Co 2p1/2 binding energy	796.4 eV	—	—	Text Exact Reported	139 · 3.1 · Fig. 3D
Co 2p3/2 binding energy	780.6 eV	—	—	Text Exact Reported	139 · 3.1 · Fig. 3D
Co 2p shake-up satellite	784.6 eV	—	—	Text Exact Reported	139 · 3.1 · Fig. 3D
O 1s carboxyl peak	531.7 eV	—	—	Text Exact Reported	139 · 3.1 · Fig. 3B
O 1s hydroxyl peak	533.5 eV	—	—	Text Exact Reported	139 · 3.1 · Fig. 3B