Microscopy Morphology — Controlling the Thermoelectric Properties of Organometallic Coordination Polymers via Ligand Design

3 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

pristine Ni-btt freestanding pellet · Pellet

Particle size mechanically decreased to 1-10 um by ball milling; compressed into pellets at 2.6 GPa for SEM/EDS compositional mapping.

Geometry: compressed pellet
Context: pristine framework pellet
Measurement source: 3 · 2.2 Compositional and Structural Characterization · Table 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
C atomic percentage	66.0	—	—	Table Exact Reported	3 · 2.2 · Table 1
Ni atomic percentage	6.0	—	—	Table Exact Reported	3 · 2.2 · Table 1
S atomic percentage	20.7	—	—	Table Exact Reported	3 · 2.2 · Table 1
S/Ni ratio	3.5 (theoretical 4)	—	—	Table Exact Reported	3 · 2.2 · Table 1

pristine Ni-diett freestanding pellet · Pellet

Particle size mechanically decreased to 1-10 um by ball milling; compressed into pellets at 2.6 GPa for SEM/EDS compositional mapping.

Geometry: compressed pellet
Context: pristine framework pellet
Measurement source: 3 · 2.2 Compositional and Structural Characterization · Table 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
C atomic percentage	51.2	—	—	Table Exact Reported	3 · 2.2 · Table 1
Ni atomic percentage	5.7	—	—	Table Exact Reported	3 · 2.2 · Table 1
S atomic percentage	37.5	—	—	Table Exact Reported	3 · 2.2 · Table 1
S/Ni ratio	6.6 (theoretical 8)	—	—	Table Exact Reported	3 · 2.2 · Table 1

pristine Ni-ett freestanding pellet · Pellet

Particle size mechanically decreased to 1-10 um by ball milling; compressed into pellets at 2.6 GPa for SEM/EDS compositional mapping.

Geometry: compressed pellet
Context: pristine framework pellet
Measurement source: 3 · 2.2 Compositional and Structural Characterization · Table 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
C atomic percentage	41.4	—	—	Table Exact Reported	3 · 2.2 · Table 1
Ni atomic percentage	11.7	—	—	Table Exact Reported	3 · 2.2 · Table 1
S atomic percentage	32.2	—	—	Table Exact Reported	3 · 2.2 · Table 1
S/Ni ratio	2.6 (theoretical 4)	—	—	Table Exact Reported	3 · 2.2 · Table 1