Other — Controlling the Thermoelectric Properties of Organometallic Coordination Polymers via Ligand Design

Measurement evidence

Other

Controlling the Thermoelectric Properties of Organometallic Coordination Polymers via Ligand Design · Liu Z., Liu T., Savory C.N. et al. · Advanced Functional Materials · 2020 · 2003106

4 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Pellet fabrication protocol

pristine Ni-ett freestanding pellet · Pellet

Typical protocol for all OMCP pellets: 200 mg powder, ball milling, KBr die pressing at about 2.6 GPa.

Context
pristine purified pellets
Measurement source
5 · OMCP Pellet Fabrication
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Thermogravimetric analysis (TGA)

purified Ni-btt powder · Powder

TA Q500 under nitrogen; 293-1073 K at 20 K min-1.

Atmosphere
nitrogen
Context
pristine purified powder
Measurement source
2 · General Experimental / Figure S20 · Figure S20
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-btt thermal decomposition onsetaround 300 degCText
Approximate
7 · 2.4 Thermoelectric Characterization · Figure S20

Thermogravimetric analysis (TGA)

purified Ni-diett powder · Powder

TA Q500 under nitrogen; 293-1073 K at 20 K min-1.

Atmosphere
nitrogen
Context
pristine purified powder
Measurement source
2 · General Experimental / Figure S20 · Figure S20
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-diett thermal decomposition onsetaround 300 degCText
Approximate
7 · 2.4 Thermoelectric Characterization · Figure S20

Thermogravimetric analysis (TGA)

purified Ni-ett powder · Powder

TA Q500 under nitrogen; 293-1073 K at 20 K min-1.

Atmosphere
nitrogen
Context
pristine purified powder
Measurement source
2 · General Experimental / Figure S20 · Figure S20
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-ett thermal decomposition onsetaround 250 degCText
Approximate
7 · 2.4 Thermoelectric Characterization · Figure S20
Weight loss before decomposition<3%Text
Approximate
7 · 2.4 Thermoelectric Characterization · Figure S20