Diffraction Structure — Pd-Embedded Ti Metal–Organic Framework Nanostructures for Photocatalytic Reductive N-Formylation of Nitroarenes in Water

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Pd1.5%/Ti-MOF · Powder

PXRD of Pd/Ti-MOF loading series compared with Ti-MOF.

Context: Pd/Ti-MOF composite samples
Measurement source: p003 / article p466 · Physicochemical Characterization · Figure 1a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Pd incorporation effect on PXRD	Pd NP incorporation did not change the Ti-MOF PXRD pattern	—	—	Text Qualitative	p002-p003 / article pp465-466 · Physicochemical Characterization · Figure 1a

Ti-MOF · Powder

PXRD pattern compared with simulated Ti-MOF pattern/card no. 7211159.

Context: pristine control
Measurement source: p002-p003 / article pp465-466 · Physicochemical Characterization · Figure 1a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ti-MOF PXRD phase match	matches simulated Ti-MOF pattern (card no. 7211159)	—	—	Text Qualitative	p002-p003 / article pp465-466 · Physicochemical Characterization · Figure 1a

spent Pd1.5%/Ti-MOF after recycling · Powder

Spent Pd1.5%/Ti-MOF after recycling compared with fresh catalyst.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Spent Pd1.5%/Ti-MOF PXRD match to fresh catalyst	spent and fresh PXRD patterns well matched	—	—	Text Qualitative	p010 / SI pS10 · Figure S9 · Figure S9
Spent Pd1.5%/Ti-MOF surface morphology retention	spent surface morphology well matched with fresh catalyst	—	—	Text Qualitative	p010 / SI pS10 · Figure S9 · Figure S9