Microscopy Morphology — Pd-Embedded Ti Metal–Organic Framework Nanostructures for Photocatalytic Reductive N-Formylation of Nitroarenes in Water

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Pd1.5%/Ti-MOF · Powder

Morphology after Pd incorporation.

Context: Pd/Ti-MOF composite compared with pristine Ti-MOF
Measurement source: p003-p004 / article pp466-467 · Physicochemical Characterization · Figure 2c,d

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Pd1.5%/Ti-MOF morphology retained	original morphology did not change after Pd incorporation	—	—	Text Qualitative	p004 / article p467 · Physicochemical Characterization · Figure 2c,d

Ti-MOF · Powder

Morphology at 40k and 100k magnification.

Context: pristine control
Measurement source: p003 / article p466 · Physicochemical Characterization · Figure 2a,b

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ti-MOF morphology	rectangular and square-shaped tetragonal nanoplate morphology	—	—	Text Qualitative	p003 / article p466 · Physicochemical Characterization · Figure 2a,b

Pd1.5%/Ti-MOF · Powder

TEM and HR-TEM imaging of Pd1.5%/Ti-MOF.

Context: target composite
Measurement source: p004 / article p467 · Physicochemical Characterization · Figure 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Pd NP distribution	homogeneous distribution of ultrasmall Pd NPs over the Ti-MOF	—	—	Text Qualitative	p004 / article p467 · Physicochemical Characterization · Figure 3e,f
Pd NP lattice fringe spacing	0.22 nm corresponding to the (111) plane of Pd NPs	—	—	Text Exact Reported	p004 / article p467 · Physicochemical Characterization · Figure S1 referenced