cMOF Evidence Base

Synthesis evidence

Self-Powered Disinfection Using Triboelectric, Conductive Wires of Metal-Organic Frameworks

Huo Z.-Y., Yang Y., Jeong J.-M. et al. · Nano Letters · 2023 · 3090-3097

5 structured synthesis routes

Completeness describes how fully the route could be reconstructed from the main article and supporting information.

Partial recipeSource: SI

Route 1: Solvothermal

SI p002 · Electrode Preparation · Figure S8

Metal precursorsCu(OH)2 NP-modified Cu mesh
Linker precursorsHHTP (0.02 mM)
Solventswater/DMF, v:v = 1:1
Atmosphereair / not otherwise specified
Temperature85
Time0.5
Substrate orientationCu(OH)2 NP-modified Cu mesh immersed in HHTP water/DMF solution
Oxidant / reductantCu(OH)2 nanoparticle precursor generated by APS oxidation
Work-upnot reported
Activationnot reported
Show 3 structured reagent records
RoleReagentAmount / concentrationSource
Metal SourceCu(OH)2 NP-modified Cu meshNot specifiedSI p002 · Electrode Preparation · Figure S8
LinkerHHTP0.02 mMSI p002 · Electrode Preparation · Figure S8
Solventwater/DMFv:v = 1:1SI p002 · Electrode Preparation · Figure S8
Partial recipeSource: Both

Route 2: Solvothermal

SI p002 · Electrode Preparation · Figure S3

Metal precursorsCu(OH)2 NW-Cu electrode; Cu ions from copper hydroxide nanowire precursor
Linker precursorsHHTP (0.02 mM)
Solventswater/DMF, v:v = 1:1
Atmosphereair / not otherwise specified
Temperature85
Time0.5
Substrate orientationCu(OH)2 NW-modified Cu mesh immersed in HHTP water/DMF solution
Oxidant / reductantCu(OH)2 precursor generated by APS oxidation
Work-upnot reported
Activationnot reported
Scalability contextMain text describes an enlarged 15 cm x 15 cm Cu-HHTP NW-Cu electrode for the prototype but does not give scaled reagent volumes.
Show 3 structured reagent records
RoleReagentAmount / concentrationSource
Metal SourceCu(OH)2 NW-modified Cu meshNot specifiedSI p002 · Electrode Preparation · Figure S3
LinkerHHTP0.02 mMSI p002 · Electrode Preparation · Figure S3
Solventwater/DMFv:v = 1:1SI p002 · Electrode Preparation · Figure S3
Partial recipeSource: SI

Route 3: Other

SI p002 · Electrode Preparation

Metal precursorspristine Cu mesh as copper source/substrate
Solventswater
Additives40 mM NaOH
Atmosphereair / not otherwise specified
Temperatureroom temperature
Time0.1667
Substrate orientationcopper mesh immersed in solution
Oxidant / reductant2 mM APS oxidant
Work-upnot reported
Activationnot reported
Show 4 structured reagent records
RoleReagentAmount / concentrationSource
Metal Sourcepristine Cu meshNot specifiedSI p002 · Electrode Preparation
OxidantAPS2 mMSI p002 · Electrode Preparation
BaseNaOH40 mMSI p002 · Electrode Preparation
SolventwaterNot specifiedSI p002 · Electrode Preparation
Partial recipeSource: SI

Route 4: Other

SI p002 · Electrode Preparation

Metal precursorspristine Cu mesh as copper source/substrate
Solventswater
Additives40 mM NaOH
Atmosphereair / not otherwise specified
Temperatureroom temperature
Time0.5
Substrate orientation100-mesh copper mesh immersed in solution
Oxidant / reductant2 mM ammonium peroxydisulfate (APS) oxidant
Work-upnot reported
Activationnot reported
Show 4 structured reagent records
RoleReagentAmount / concentrationSource
Metal Sourcepristine Cu meshNot specifiedSI p002 · Electrode Preparation
OxidantAPS2 mMSI p002 · Electrode Preparation
BaseNaOH40 mMSI p002 · Electrode Preparation
SolventwaterNot specifiedSI p002 · Electrode Preparation
Partial recipeSource: Both

Route 5: Other

SI p003 · TENG Fabrication and Characterization · Figure S1

Metal precursorsCu electrodes
AdditivesCCTO particles mixed with BMF solution
Atmosphereair / not specified
Temperature180
Time2
Substrate orientationCCTO-BMF coated on stator surface using automatic bar coater; rotator on FR-4 substrate
Work-upannealed at 180 deg C for 2 h
Scalability contextTENG was later integrated with a commercial turbocharger for gravity-driven prototype operation.
Show 3 structured reagent records
RoleReagentAmount / concentrationSource
OtherBMF solutionNot specifiedSI p003 · TENG Fabrication and Characterization · Figure S1
AdditiveCCTO particlesNot specifiedSI p003 · TENG Fabrication and Characterization · Figure S1
OtherCu electrodes90 pairs on stator; 90 separate on rotatorSI p003 · TENG Fabrication and Characterization · Figure S1