Diffraction Structure — Efficient MOF-Sensitized Solar Cells Featuring Solvothermally Grown [100]-Oriented Pillared Porphyrin Framework-11 Films on ZnO/FTO Surfaces

Measurement evidence

Diffraction Structure

Efficient MOF-Sensitized Solar Cells Featuring Solvothermally Grown [100]-Oriented Pillared Porphyrin Framework-11 Films on ZnO/FTO Surfaces · Gordillo M.A., Panda D.K., Saha S. · ACS Applied Materials and Interfaces · 2019 · 3196-3206

3 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction (PXRD)

bulk PPF-11 crystals · Single Crystal

Cu Kalpha radiation, Rigaku Ultima IV; as-synthesised crystals

Context
pristine PPF-11 bulk
Measurement source
3198 · Bulk PPF-11 synthesis and characterization · Figure 1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
bulk preferred orientation[001] directionQualitative
Qualitative
3198 · Bulk PPF-11 synthesis and characterization · Figure 1b
bulk PPF-11 PXRD low-angle peak2theta = 12.6Text
Rounded Reported
3198 · Bulk PPF-11 synthesis and characterization · Figure 1b
bulk PPF-11 PXRD low-angle peak2theta = 18.9Text
Rounded Reported
3198 · Bulk PPF-11 synthesis and characterization · Figure 1b
bulk PPF-11 PXRD low-angle peak2theta = 6.3Text
Rounded Reported
3198 · Bulk PPF-11 synthesis and characterization · Figure 1b

PXRD after C60 infiltration

C60-doped PPF-11 crystals · Powder

C60-doped PPF-11 compared with undoped/bulk and films

Context
guest-loaded framework structure
Measurement source
3201 · Doping PPF-11 with C60 · Figure S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD after C60 infiltrationmostly unchanged; structure and crystallinity largely intactText
Qualitative
3201 · Doping PPF-11 with C60 · Figure S6

PXRD

[100]-oriented PPF-11 film on TCPP-coated ZnO-FTO · Electrode

Solvothermally grown PPF-11/ZnO film on ZnO-FTO

Context
pristine film on ZnO-FTO
Measurement source
3199 · Spontaneous solvothermal growth · Figure 1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
film preferred orientation[100] oriented PPF-11 filmQualitative
Qualitative
3199 · Spontaneous solvothermal growth · Figure 1b
film PXRD [100] peak2theta about 15Text
Approximate
3199 · Spontaneous solvothermal growth · Figure 1b
film PXRD [100] peak2theta about 22.5Text
Approximate
3199 · Spontaneous solvothermal growth · Figure 1b
film PXRD [100] peak2theta about 30Text
Approximate
3199 · Spontaneous solvothermal growth · Figure 1b
film PXRD [100] peak2theta about 7.5Text
Approximate
3199 · Spontaneous solvothermal growth · Figure 1b