Spectroscopy — Intercatenated Coordination Polymers (ICPs) of Carboxylato Bridged Zn(II)-Isoniazid and Their Electrical Conductivity

Measurement evidence

Spectroscopy

Intercatenated Coordination Polymers (ICPs) of Carboxylato Bridged Zn(II)-Isoniazid and Their Electrical Conductivity · Naskar K., Dey A., Dutta B. et al. · Crystal Growth and Design · 2017 · 3267-3276

2 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR spectroscopy and thermogravimetric analysis

Colourless block-shaped crystals of [Zn(INH)(succ)]n (1) · Single Crystal

KBr FTIR; TGA under N2 at 10 C/min from 30-500 C.

Atmosphere
Nitrogen for TGA
Context
pristine frameworks 1-3
Measurement source
main p.3 · Materials and Physical Methods · SI Figures S1-S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
thermal stability temperature of 1240 C513.15 KText
Rounded Reported
main p.3 · Synthesis and Formulation · SI Figure S6
thermal stability temperature of 2270 C543.15 KText
Rounded Reported
main p.3 · Synthesis and Formulation · SI Figure S6
thermal stability temperature of 3Marked as a best value within this paper350 C623.15 KText
Rounded Reported
main p.3 · Synthesis and Formulation · SI Figure S6

UV-vis absorption spectroscopy and Tauc analysis

ITO/1/Al Schottky thin-film device · Thin Film

Thin films of 1, 2, and 3 prepared from well-dispersed DMSO solutions; Shimadzu 2401 PC, 200-900 nm.

Geometry
deposited thin films
Context
pristine framework thin films
Measurement source
main p.4-main p.5 · UV-vis Spectroscopy, Band Gap, and Dielectric Measurements · Figure 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Tauc optical band gap of 1Marked as a best value within this paper3.39 eVText
Rounded Reported
main p.4 · UV-vis Spectroscopy · Figure 3
Tauc optical band gap of 24.09 eVText
Rounded Reported
main p.4 · UV-vis Spectroscopy · Figure 3
Tauc optical band gap of 33.98 eVText
Rounded Reported
main p.4 · UV-vis Spectroscopy · Figure 3
UV absorption energy onset/peak of 1360 nmText
Rounded Reported
main p.4 · UV-vis Spectroscopy · Figure 3
UV absorption energy onset/peak of 2310 nmText
Rounded Reported
main p.4 · UV-vis Spectroscopy · Figure 3
UV absorption energy onset/peak of 3320 nmText
Rounded Reported
main p.4 · UV-vis Spectroscopy · Figure 3