Measurement evidence
Highly Porous, Electrically Conductive Two-Dimensional Nickel–Hexaaminodehydrobenzoannulene Frameworks · Ohkubo E., Suzuki M., Aizawa N. et al. · Journal of the American Chemical Society · 2025 · 31940-31951
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Ni3(HI12)2 film on interdigitated Au electrodes · Thin Film
beamline BL19B2 at SPring-8; 12.398 keV, incident angle 0.12 deg; 30 s exposure
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| film packing compared with powder | film packing structures identical to corresponding powder samples | — | — | Text Qualitative | S27-S28 · S2-13 · Figure S23 |
Ni3(HI18)2 film on interdigitated Au electrodes · Thin Film
beamline BL19B2 at SPring-8; 12.398 keV, incident angle 0.12 deg; 30 s exposure
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| film packing compared with powder | film packing structures identical to corresponding powder samples | — | — | Text Qualitative | S27-S28 · S2-13 · Figure S23 |
Ni3(HITP)2 film on interdigitated Au electrodes · Thin Film
beamline BL19B2 at SPring-8; 12.398 keV, incident angle 0.12 deg; 30 s exposure
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| film packing compared with powder | film packing structures identical to corresponding powder samples | — | — | Text Qualitative | S27-S28 · S2-13 · Figure S23 |
Ni3(HI12)2 activated powder · Powder
Cu Kalpha, 2theta 1-30 deg, P6/mmm AA-stacking model refinement
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| a=b lattice parameter | 2.68 nm (26.78 A in SI Table S3) | — | — | SI Table Exact Reported | S17 · S2-4 · Table S3 |
| c lattice parameter | 0.333 nm (3.33 A) | — | — | SI Table Exact Reported | S17 · S2-4 · Table S3 |
| 100 peak FWHM | 0.51 deg | — | — | Text Rounded Reported | 31944 · Preparation and Structure of MOFs · Figure 2b |
| Rwp AA refinement | 11.3% | — | — | SI Table Exact Reported | S17 · S2-4 · Table S3 |
Ni3(HI18)2 activated powder · Powder
Cu Kalpha, 2theta 1-30 deg, P6/mmm AA-stacking model refinement
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| a=b lattice parameter | 3.19 nm (31.86 A in SI Table S3) | — | — | SI Table Exact Reported | S17 · S2-4 · Table S3 |
| c lattice parameter | 0.331 nm (3.31 A) | — | — | SI Table Exact Reported | S17 · S2-4 · Table S3 |
| 100 peak FWHM | 0.40 deg | — | — | Text Rounded Reported | 31944 · Preparation and Structure of MOFs · Figure 2c |
| Rwp AA refinement | 10.5% | — | — | SI Table Exact Reported | S17 · S2-4 · Table S3 |
Ni3(HITP)2 activated powder · Powder
Cu Kalpha, 2theta 1-30 deg, P6/mmm AA-stacking model refinement
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| a=b lattice parameter | 2.68 nm (21.74 A in SI Table S3) | — | — | Text Rounded Reported | 31943 · Preparation and Structure of MOFs · Figure 2; Table S3 |
| c lattice parameter | 0.33 nm (3.32 A in SI Table S3) | — | — | Text Rounded Reported | 31943 · Preparation and Structure of MOFs · Figure 2; Table S3 |
| 100 peak FWHM | 0.42 deg | — | — | Text Rounded Reported | 31944 · Preparation and Structure of MOFs · Figure 2a |
| Rwp AA refinement | 12.9% | — | — | SI Table Exact Reported | S17 · S2-4 · Table S3 |