Diffraction Structure — Structural and electronic modulation of conductive MOFs for efficient oxygen evolution reaction electrocatalysis

Measurement evidence

Diffraction Structure

Structural and electronic modulation of conductive MOFs for efficient oxygen evolution reaction electrocatalysis · Li J., Liu P., Mao J. et al. · Journal of Materials Chemistry A · 2021 · 11248-11254

3 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction (PXRD)

NiPc-NiFex powder series · Powder

PANalytical Empyrean, Cu Kalpha radiation, 40 kV and 40 mA; compared with simulated pattern.

Measurement source
2 · Synthesis and characterization · Fig. S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD peak assigned to (001)around 26.3 degreesText
Approximate
2 · Synthesis and characterization · Fig. S2
PXRD peak assigned to (100)around 5.5 degreesText
Approximate
2 · Synthesis and characterization · Fig. S2
PXRD peak assigned to (200)around 10.5 degreesText
Approximate
2 · Synthesis and characterization · Fig. S2

PXRD

NiPc-Fe powder control · Powder

PXRD pattern of NiPc-Fe control.

Measurement source
3 · Synthesis and characterization · Fig. S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
NiPc-Fe diffraction peaksNo diffraction peaks observedText
Qualitative
3 · Synthesis and characterization · Fig. S3

PXRD

NiPc-Ni powder control · Powder

Experimental and simulated PXRD pattern of NiPc-Ni MOF.

Measurement source
3 · PXRD Patterns · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
NiPc-Ni experimental/simulated PXRD comparisonExperimental and simulated PXRD pattern shownCaption
Qualitative
3 · PXRD Patterns · Figure S1