Microscopy Morphology — Structural and electronic modulation of conductive MOFs for efficient oxygen evolution reaction electrocatalysis

Measurement evidence

Microscopy Morphology

Structural and electronic modulation of conductive MOFs for efficient oxygen evolution reaction electrocatalysis · Li J., Liu P., Mao J. et al. · Journal of Materials Chemistry A · 2021 · 11248-11254

3 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM and TEM

NiPc-Fe powder control · Powder

SEM and TEM morphology of NiPc-Fe control.

Measurement source
3 · Synthesis and characterization · Fig. S3, Fig. S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
NiPc-Fe morphologyirregular particles with smooth surface; particles stacked by nanosheetsText
Qualitative
3 · Synthesis and characterization · Fig. S4g,h

SEM, TEM and TEM-EDX

NiPc-NiFex powder series · Powder

SEM/TEM used to examine morphology of NiPc-NiFe0.05, NiPc-NiFe0.09 and NiPc-NiFe0.20; EDX mapping for NiPc-NiFe0.09.

Measurement source
2 · Synthesis and characterization · Fig. 2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
NiPc-NiFe0.09 elemental mappinghomogeneous presence of all elements; Fe sites evenly dispersedQualitative
Qualitative
2 · Synthesis and characterization · Fig. 2g
NiPc-NiFe0.20 crystallite size100 nm crystallitesText
Rounded Reported
2 · Synthesis and characterization · Fig. 2
NiPc-NiFe0.05 SEM cube size range100-500 nmText
Range
2 · Synthesis and characterization · Fig. 2
NiPc-NiFe0.09 SEM cube size range100-500 nmText
Range
2 · Synthesis and characterization · Fig. 2