Spectroscopy — Structural and electronic modulation of conductive MOFs for efficient oxygen evolution reaction electrocatalysis

4 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

NiPc-NiFe0.05 powder · Powder

Survey and high-resolution XPS spectra for NiPc-NiFe0.05.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
NiPc-NiFe0.05 C=O:C-O integral ratio	47:53	—	—	Caption Exact Reported	6 · XPS Spectra · Figure S6

NiPc-NiFe0.09 powder · Powder

Survey and high-resolution XPS spectra for NiPc-NiFe0.09.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni 2p1/2 peak in NiPc-NiFex	873.0 eV	—	—	Text Exact Reported	2 · Synthesis and characterization · Fig. 3
Ni 2p3/2 peak in NiPc-NiFex	855.8 eV	—	—	Text Exact Reported	2 · Synthesis and characterization · Fig. 3
NiPc-NiFe0.09 C=O:C-O integral ratio	55:45	—	—	Caption Exact Reported	6 · XPS Spectra · Figure S5

NiPc-NiFe0.20 powder · Powder

Survey and high-resolution XPS spectra for NiPc-NiFe0.20.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
NiPc-NiFe0.20 C=O:C-O integral ratio	51:49	—	—	Caption Exact Reported	7 · XPS Spectra · Figure S7

NiPc-Fe powder control · Powder

Survey and high-resolution XPS spectra for NiPc-Fe.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
NiPc-Fe Fe(II) Fe 2p subpeak	710.0 eV	—	—	Text Exact Reported	3 · Synthesis and characterization · Fig. S8f
NiPc-Fe Fe(III) Fe 2p subpeak	712.2 eV	—	—	Text Exact Reported	3 · Synthesis and characterization · Fig. S8f
NiPc-Fe C=O:C-O integral ratio	56:44	—	—	Caption Exact Reported	7 · XPS Spectra · Figure S8