Diffraction Structure — Processable UiO-66 Metal-Organic Framework Fluid Gel and Electrical Conductivity of Its Nanofilm with Sub-100 nm Thickness

Measurement evidence

Diffraction Structure

Processable UiO-66 Metal-Organic Framework Fluid Gel and Electrical Conductivity of Its Nanofilm with Sub-100 nm Thickness · Somjit V., Thinsoongnoen P., Waiprasoet S. et al. · ACS Applied Materials and Interfaces · 2021 · 30844-30852

4 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

GIXRD and SEM

MOF-801 thin film · Thin Film

MOF-801 fluid gel/film characterised after applying UiO-66 spin-coating parameters.

Geometry
thin film on glass
Context
pristine MOF-801 generality sample
Measurement source
p005 / 30848 · Results and Discussion · Figure 4c; Figure S6a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
MOF-801 film morphologysmooth surface by SEMText
Qualitative
p005 / 30848 · Results and Discussion · Figure 4c
MOF-801 structure after fluid-gel processingstructure preserved in fluid gel state by GIXRDText
Qualitative
p005 / 30848 · Results and Discussion · Figure S6a

GIXRD and SEM

MOF-808 thin film · Thin Film

MOF-808 fluid gel/film characterised after applying UiO-66 spin-coating parameters.

Geometry
thin film on glass
Context
pristine MOF-808 generality sample
Measurement source
p005 / 30848 · Results and Discussion · Figure 4d; Figure S6b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
MOF-808 film morphologysmooth surface by SEMText
Qualitative
p005 / 30848 · Results and Discussion · Figure 4d
MOF-808 structure after fluid-gel processingstructure preserved in fluid gel state by GIXRDText
Qualitative
p005 / 30848 · Results and Discussion · Figure S6b

GIXRD before and after chronoamperometry

60 nm UiO-66 nanofilm · Thin Film

60 nm UiO-66 thin film before device fabrication and after chronoamperometry measurement for 3600 s.

Geometry
60 nm UiO-66 film/device
Context
pristine UiO-66 nanofilm stability check
Measurement source
p007 / SI p7 · Supporting Information · Figure S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
GIXRD structural stability after chronoamperometrycorresponded peak retained before and after 3600 s chronoamperometryText
Qualitative
p006 / 30849 · Results and Discussion · Figure S14

XRD/GIXRD using Bruker D8 ADVANCE, Cu Kalpha radiation

UiO-66 nanofilm thickness series · Thin Film

Thin films and fluid gels measured by GIXRD with grazing incidence angle 0.10 degrees, 4 s step^-1, 0.01 degree step.

Geometry
thin films on glass
Context
pristine UiO-66 fluid gel and thin films
Measurement source
p002-p004 / 30845-30847 · Materials and Methods; Results and Discussion · Figure 3c; Figure S5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
defect-site-associated diffraction peak2theta = 12.0 degreesText
Rounded Reported
p004 / 30847 · Results and Discussion · Figure 3c
UiO-66 fluid-gel crystallite size by GIXRD Scherrer equation10 nmText
Rounded Reported
p004 / 30847 · Results and Discussion · Figure 3d
UiO-66 (111) d-spacing range11.5-12.0 AText
Range
p004 / 30847 · Results and Discussion · Figure 3c
major UiO-66 diffraction peak2theta = 7.4 degrees indexed as (111)Text
Rounded Reported
p004 / 30847 · Results and Discussion · Figure 3c