Porosity — Processable UiO-66 Metal-Organic Framework Fluid Gel and Electrical Conductivity of Its Nanofilm with Sub-100 nm Thickness

Measurement evidence

Porosity

Processable UiO-66 Metal-Organic Framework Fluid Gel and Electrical Conductivity of Its Nanofilm with Sub-100 nm Thickness · Somjit V., Thinsoongnoen P., Waiprasoet S. et al. · ACS Applied Materials and Interfaces · 2021 · 30844-30852

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 adsorption-desorption with BET and NLDFT analysis

Gas sorption and porosity

UiO-66 fluid gel · Unknown

MicrotracBEL BELSORP-mini II at -196 C; samples degassed at 150 C under vacuum for 24 h before adsorption.

Temperature: 77
Atmosphere: N2 adsorption
Context: pristine UiO-66 fluid gel compared with microcrystalline UiO-66 powder
Measurement source: p002,p004 / 30845,30847 · Materials and Methods; Results and Discussion · Figure S3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
BET surface area	1052 m2 g-1	—	—	Text Exact Reported	p004 / 30847 · Results and Discussion · Figure S3
additional mesopore average size	2.7 nm	—	—	Text Exact Reported	p004 / 30847 · Results and Discussion · Figure S3
average micropore size	1.4 nm	—	—	Text Exact Reported	p004 / 30847 · Results and Discussion · Figure S3
total pore volume	1.63 cm3 g-1	—	—	Text Exact Reported	p004 / 30847 · Results and Discussion · Figure S3

Water adsorption isotherm

Gas sorption and porosity

UiO-66 fluid gel · Unknown

MicrotracBEL BELSORP-max at 25 C; degassed at 150 C under vacuum for 24 h before adsorption.

Temperature: 298
Atmosphere: water vapour adsorption
Context: pristine UiO-66 fluid gel compared with microcrystalline powder
Measurement source: p002-p003 / 30845-30846 · Materials and Methods; Results and Discussion · Figure S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
water uptake relative to powder	4 times higher uptake than UiO-66 powder	—	—	Text Rounded Reported	p003 / 30846 · Results and Discussion · Figure S1