Measurement evidence
Upgrading Structural Conjugation in Three-Dimensional Ni-Based Metal-Organic Frameworks for Promoting Electrical Conductivity and Specific Capacitance · Tai H., Ding W., Zhang X. et al. · Inorganic Chemistry · 2024 · 18083-18091
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
as-synthesised Ni-BPE crystals · Single Crystal
PANalytical EMPYREAN; Cu Kalpha; 2theta 5-50 degrees
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PXRD phase/crystallinity assignment | experimental PXRD agreed well with simulated pattern | — | — | Text Qualitative | p. 18087 · XPS, PXRD, IR, and TGA Characterization · Figure 2a |
as-synthesised Ni-BPY crystals · Single Crystal
PANalytical EMPYREAN; Cu Kalpha; 2theta 5-50 degrees
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PXRD phase/crystallinity assignment | experimental PXRD agreed well with simulated pattern | — | — | Text Qualitative | p. 18087 · XPS, PXRD, IR, and TGA Characterization · Figure 2a |
as-synthesised Ni-BPE crystals · Single Crystal
Bruker APEX-II CCD; graphite-monochromic Mo Kalpha radiation, lambda = 0.71073 A; data collected at 273.15 K; structure refined with SHELXTL-97/OLEX-2
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Ni-BPE unit-cell a | 16.7465(10) A | — | — | SI Table Exact Reported | S2 · Table S1 · Table S1 |
| Ni-BPE unit-cell b | 16.7465(10) A | — | — | SI Table Exact Reported | S2 · Table S1 · Table S1 |
| Ni-BPE unit-cell c | 13.5599(9) A | — | — | SI Table Exact Reported | S2 · Table S1 · Table S1 |
| Ni-BPE unit-cell volume | 3293.3(4) A3 | — | — | SI Table Exact Reported | S2 · Table S1 · Table S1 |
| Ni-BPE unit-cell z | 6 | — | — | SI Table Exact Reported | S2 · Table S1 · Table S1 |
| Ni-BPE empirical formula | C21H13N4NiO6 | — | — | SI Table Exact Reported | S2 · Table S1 · Table S1 |
| Ni-BPE Ni-N bond length | 1.929 A | — | — | SI Table Exact Reported | S3 · Table S2 · Table S2 |
| Ni-BPE Ni-O bond length maximum | 2.109 A | — | — | SI Table Exact Reported | S3 · Table S2 · Table S2 |
| Ni-BPE Ni-O bond length minimum | 2.060 A | — | — | SI Table Exact Reported | S3 · Table S2 · Table S2 |
| Ni-BPE space group | P-3c1 | — | — | SI Table Exact Reported | S2 · Table S1 · Table S1 |