Electrochemistry Application — Electrochemical deposition of Cu metal-organic framework films for the dual analysis of pathogens

Measurement evidence

Electrochemistry Application

Electrochemical deposition of Cu metal-organic framework films for the dual analysis of pathogens · Sun Z., Peng Y., Wang M. et al. · Analytical Chemistry · 2020

6 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

cyclic voltammetry

Cu-MOF/GCE electrode · Electrode

CV in 0.1 M KCl used to optimise Cu-MOF deposition potential and deposition time.

Geometry
Cu-MOF film on GCE
Context
pristine_control
Measurement source
main p.5, article p.8999 · Optimization of Experimental Conditions · Figure S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
selected Cu-MOF electrodeposition potentialMarked as a best value within this paper-1.3 VText
Exact Reported
main p.5, article p.8999 · Optimization of Experimental Conditions · Figure S2A
selected Cu-MOF electrodeposition timeMarked as a best value within this paper5 min0.0833333333 hText
Exact Reported
main p.5, article p.8999 · Optimization of Experimental Conditions · Figure S2B

differential pulse voltammetry

AuNPs/Cu-MOF/GCE electrode · Electrode

DPV in Fe(CN)6 redox electrolyte; 50 mV/s sweep, 50 ms pulse width, 0.2 s pulse period, voltage range reported as -0.2 to -0.6 V.

Geometry
three-electrode cell
Context
composite compared with bare and pristine MOF controls
Measurement source
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2B
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
AuNPs/Cu-MOF/GCE DPV peak currentabout 100 uA from Figure 2BFigure Axis
Approximate
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2B
bare GCE DPV peak currentabout 75 uA from Figure 2BFigure Axis
Approximate
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2B
MOF/GCE DPV peak currentabout 88 uA from Figure 2BFigure Axis
Approximate
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2B

electrochemical impedance spectroscopy

AuNPs/Cu-MOF/GCE electrode · Electrode

EIS of AuNPs/Cu-MOF/GCE in Fe(CN)6 redox electrolyte.

Geometry
three-electrode cell
Context
composite
Measurement source
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2A
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
AuNPs/Cu-MOF EIS behaviourimpedance spectrum similar to a straight lineText
Qualitative
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2A

electrochemical impedance spectroscopy

bare GCE · Electrode

EIS in 5 mM [Fe(CN)6]3-/4- with 1 M KCl; 5 mV amplitude, 0.224 V bias, 0.1-10 kHz.

Geometry
three-electrode cell; SCE reference; Pt counter
Context
bare control
Measurement source
main p.3, article p.8996 · Electrochemical Measurements · Figure 2A
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
bare GCE impedance semicircle diameteralmost 180 ohmText
Approximate
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2A

electrochemical impedance spectroscopy

Cu-MOF/GCE electrode · Electrode

EIS of Cu-MOF/GCE in Fe(CN)6 redox electrolyte under the same conditions as bare GCE.

Geometry
three-electrode cell
Context
pristine_control
Measurement source
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2A
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-MOF/GCE impedanceMarked as a best value within this paper50 ohmText
Rounded Reported
main p.4, article p.8997 · Feasibility of the Biosensor · Figure 2A

electrochemical impedance spectroscopy

DNA/AuNPs/Cu-MOF/GCE biosensor · Electrode

EIS of DNA/AuNPs/Cu-MOF/GCE before target exposure.

Geometry
aptamer-modified three-electrode biosensor
Context
composite
Measurement source
main p.4, article p.8998 · Feasibility of the Biosensor · Figure 3A
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
DNA/AuNPs/Cu-MOF/GCE electron-transfer resistance560 ohmText
Rounded Reported
main p.4, article p.8998 · Feasibility of the Biosensor · Figure 3A