Microscopy Morphology — Radiation-Induced in Situ Construction of 2D Conductive Defect-Rich Metal-Organic Frameworks for High-Performance Supercapacitor

Measurement evidence

Microscopy Morphology

Radiation-Induced in Situ Construction of 2D Conductive Defect-Rich Metal-Organic Frameworks for High-Performance Supercapacitor · Zhang K., Mao X., Yan W. et al. · Small · 2025 · e07135

2 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FE-SEM, HR-TEM, SAED and TEM-EDS

Cu-CAT-Rad · Powder

Morphology, 100-facet lattice fringes, diffraction and elemental ratios

Context
pristine target framework
Measurement source
2,4 · Results and Discussion · Figure 2d-g
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
EDS C atomic proportion72.34 at%+/- 0.07SI Table
Rounded Reported
10 · Section S4 · Table S2
EDS Cu/C atomic ratio8.47+/- 0.61SI Table
Rounded Reported
10 · Section S4 · Table S2
EDS Cu atomic proportion6.13 at%+/- 0.44SI Table
Rounded Reported
10 · Section S4 · Table S2
EDS N atomic proportion2.00 +/- 0.34 at%+/- 0.34SI Table
Rounded Reported
10 · Section S4 · Table S2
EDS O atomic proportion19.53 +/- 0.71 at%+/- 0.71SI Table
Rounded Reported
10 · Section S4 · Table S2
HR-TEM 100-facet lattice fringed100 = 1.84 nmText
Rounded Reported
2 · Results and Discussion · Figure 2e

FE-SEM, HR-TEM, SAED and TEM-EDS

Cu-CAT-Sol · Powder

Morphology, 100-facet lattice fringes, diffraction and elemental ratios

Context
pristine control framework
Measurement source
2,4 · Results and Discussion · Figure 2a-c,g
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
EDS C atomic proportion76.24 at%+/- 0.71SI Table
Rounded Reported
10 · Section S4 · Table S1
EDS Cu/C atomic ratio7.72+/- 1.69SI Table
Rounded Reported
10 · Section S4 · Table S1
EDS Cu atomic proportion5.89 at%+/- 1.34SI Table
Rounded Reported
10 · Section S4 · Table S1
EDS N atomic proportion0.65 +/- 0.52 at%+/- 0.52SI Table
Rounded Reported
10 · Section S4 · Table S1
EDS O atomic proportion17.23 +/- 1.53 at%+/- 1.53SI Table
Rounded Reported
10 · Section S4 · Table S1
HR-TEM 100-facet lattice fringed100 = 1.77 nmText
Rounded Reported
2 · Results and Discussion · Figure 2b