cMOF Evidence Base
Other — Benign preparation of metal–organic frameworks of trimesic acid and Cu, Co or Ni for potential sensor applications

Measurement evidence

Other

Benign preparation of metal–organic frameworks of trimesic acid and Cu, Co or Ni for potential sensor applications · Sel K., Demirci S., Meydan E. et al. · Journal of Electronic Materials · 2015 · 136-143

3 measurement groups · 30 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis (TGA)

Thermogravimetric analysis

TMA-Co(II) powder · Powder

SII TG/DTA 6300; 3-5 mg sample, 50-1000 deg C, 10 deg C/min, N2 flow 100 mL/min.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p004-p006 · Characterization; MOF Characterization · Fig. 5; Table III
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TGA degradation step I end temperature100 deg C to 165 deg C (9.0%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step I reported percentage9.0%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step I start temperature100 deg C to 165 deg C (9.0%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step II end temperature431 deg C to 502 deg C (53.7%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step II reported percentage53.7%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step II start temperature431 deg C to 502 deg C (53.7%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step III end temperature527 deg C to 571 deg C (66.5%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step III reported percentage66.5%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step III start temperature527 deg C to 571 deg C (66.5%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step IV end temperature600 deg C to 950 deg C (72.3%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step IV reported percentage72.3%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step IV start temperature600 deg C to 950 deg C (72.3%)——Table
Range		p005-p006 · MOF Characterization · Table III

Thermogravimetric analysis (TGA)

Thermogravimetric analysis

TMA-Cu(II) powder · Powder

SII TG/DTA 6300; 3-5 mg sample, 50-1000 deg C, 10 deg C/min, N2 flow 100 mL/min.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p004-p006 · Characterization; MOF Characterization · Fig. 5; Table III
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TGA degradation step I end temperature88 deg C to 196 deg C (6.8%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step I reported percentage6.8%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step I start temperature88 deg C to 196 deg C (6.8%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step II end temperature269 deg C to 366 deg C (42.5%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step II reported percentage42.5%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step II start temperature269 deg C to 366 deg C (42.5%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step III end temperature370 deg C to 1000 deg C (56.4%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step III reported percentage56.4%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step III start temperature370 deg C to 1000 deg C (56.4%)——Table
Range		p005-p006 · MOF Characterization · Table III

Thermogravimetric analysis (TGA)

Thermogravimetric analysis

TMA-Ni(II) powder · Powder

SII TG/DTA 6300; 3-5 mg sample, 50-1000 deg C, 10 deg C/min, N2 flow 100 mL/min.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p004-p006 · Characterization; MOF Characterization · Fig. 5; Table III
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TGA degradation step I end temperature100 deg C to 155 deg C (8.9%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step I reported percentage8.9%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step I start temperature100 deg C to 155 deg C (8.9%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step II end temperature412 deg C to 486 deg C (56.3%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step II reported percentage56.3%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step II start temperature412 deg C to 486 deg C (56.3%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step III end temperature529 deg C to 950 deg C (69.5%)——Table
Range		p005-p006 · MOF Characterization · Table III
TGA degradation step III reported percentage69.5%——Table
Exact Reported		p005-p006 · MOF Characterization · Table III
TGA degradation step III start temperature529 deg C to 950 deg C (69.5%)——Table
Range		p005-p006 · MOF Characterization · Table III