Porosity — Benign preparation of metal–organic frameworks of trimesic acid and Cu, Co or Ni for potential sensor applications

Measurement evidence

Porosity

Benign preparation of metal–organic frameworks of trimesic acid and Cu, Co or Ni for potential sensor applications · Sel K., Demirci S., Meydan E. et al. · Journal of Electronic Materials · 2015 · 136-143

3 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 adsorption-desorption / BET analysis

TMA-Co(II) powder · Powder

TriStar II Micromeritics; samples kept at 50 deg C for 3 days and degassed at 80 deg C for 8 h before liquid-N2 adsorption-desorption.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p003-p005 · Pore Characteristics · Table II
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area0.11 m2/gTable
Exact Reported
p005 · MOF Characterization · Table II
Pore sizenot measured / dash in tableTable
Qualitative
p005 · MOF Characterization · Table II
Pore volumenot measured / dash in tableTable
Qualitative
p005 · MOF Characterization · Table II
Gravimetric yield45.6 +/- 10.1%10.1%Table
Exact Reported
p005 · MOF Characterization · Table II

N2 adsorption-desorption / BET analysis

TMA-Cu(II) powder · Powder

TriStar II Micromeritics; samples kept at 50 deg C for 3 days and degassed at 80 deg C for 8 h before liquid-N2 adsorption-desorption.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p003-p005 · Pore Characteristics · Table II
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface areaMarked as a best value within this paper330.64 m2/gTable
Exact Reported
p005 · MOF Characterization · Table II
Pore sizeMarked as a best value within this paper155.62 AngstromTable
Exact Reported
p005 · MOF Characterization · Table II
Pore volumeMarked as a best value within this paper0.0676 cm3/gTable
Exact Reported
p005 · MOF Characterization · Table II
Gravimetric yieldMarked as a best value within this paper67.5 +/- 5.2%5.2%Table
Exact Reported
p005 · MOF Characterization · Table II

N2 adsorption-desorption / BET analysis

TMA-Ni(II) powder · Powder

TriStar II Micromeritics; samples kept at 50 deg C for 3 days and degassed at 80 deg C for 8 h before liquid-N2 adsorption-desorption.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p003-p005 · Pore Characteristics · Table II
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area0.91 m2/gTable
Exact Reported
p005 · MOF Characterization · Table II
Pore size140.43 AngstromTable
Exact Reported
p005 · MOF Characterization · Table II
Pore volume0.0044 cm3/gTable
Exact Reported
p005 · MOF Characterization · Table II
Gravimetric yield45.9 +/- 9.6%9.6%Table
Exact Reported
p005 · MOF Characterization · Table II