Porosity — Benign preparation of metal–organic frameworks of trimesic acid and Cu, Co or Ni for potential sensor applications

Measurement evidence

Porosity

Benign preparation of metal–organic frameworks of trimesic acid and Cu, Co or Ni for potential sensor applications · Sel K., Demirci S., Meydan E. et al. · Journal of Electronic Materials · 2015 · 136-143

3 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 adsorption-desorption / BET analysis

TMA-Co(II) powder · Powder

TriStar II Micromeritics; samples kept at 50 deg C for 3 days and degassed at 80 deg C for 8 h before liquid-N2 adsorption-desorption.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p003-p005 · Pore Characteristics · Table II
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area0.11 m2/g——Table
Exact Reported
p005 · MOF Characterization · Table II
Pore sizenot measured / dash in table——Table
Qualitative
p005 · MOF Characterization · Table II
Pore volumenot measured / dash in table——Table
Qualitative
p005 · MOF Characterization · Table II
Gravimetric yield45.6 +/- 10.1%—10.1%Table
Exact Reported
p005 · MOF Characterization · Table II

N2 adsorption-desorption / BET analysis

TMA-Cu(II) powder · Powder

TriStar II Micromeritics; samples kept at 50 deg C for 3 days and degassed at 80 deg C for 8 h before liquid-N2 adsorption-desorption.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p003-p005 · Pore Characteristics · Table II
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface areaMarked as a best value within this paper330.64 m2/g——Table
Exact Reported
p005 · MOF Characterization · Table II
Pore sizeMarked as a best value within this paper155.62 Angstrom——Table
Exact Reported
p005 · MOF Characterization · Table II
Pore volumeMarked as a best value within this paper0.0676 cm3/g——Table
Exact Reported
p005 · MOF Characterization · Table II
Gravimetric yieldMarked as a best value within this paper67.5 +/- 5.2%—5.2%Table
Exact Reported
p005 · MOF Characterization · Table II

N2 adsorption-desorption / BET analysis

TMA-Ni(II) powder · Powder

TriStar II Micromeritics; samples kept at 50 deg C for 3 days and degassed at 80 deg C for 8 h before liquid-N2 adsorption-desorption.

Atmosphere
N2
Context
Pristine TMA-M powder
Measurement source
p003-p005 · Pore Characteristics · Table II
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area0.91 m2/g——Table
Exact Reported
p005 · MOF Characterization · Table II
Pore size140.43 Angstrom——Table
Exact Reported
p005 · MOF Characterization · Table II
Pore volume0.0044 cm3/g——Table
Exact Reported
p005 · MOF Characterization · Table II
Gravimetric yield45.9 +/- 9.6%—9.6%Table
Exact Reported
p005 · MOF Characterization · Table II