Measurement evidence
Thousand-fold increase in O2electroreduction rates with conductive MOFs · Mariano R.G., Wahab O.J., Rabinowitz J.A. et al. · ACS Central Science · 2022 · 975-982
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
As-synthesised Co3(HITP)2 powder · Powder
As-synthesised Co3(HITP)2 and Cu3(HITP)2 powders.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Co3(HITP)2 and Cu3(HITP)2 phase assignment | PXRD, XPS and N2 adsorption data were consistent with successful synthesis of monophasic, porous crystalline 2D MOFs. | — | — | Text Qualitative | SI p.S9 · Supplementary text 1 · Figures S12-S15 |
As-synthesised Ni3(HITP)2 powder · Powder
As-synthesised Ni3(HITP)2 powder; Bruker Advance II, Ni-filtered Cu Kalpha radiation.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Ni3(HITP)2 phase assignment | PXRD consistent with literature precedent; monophasic and highly crystalline 2D framework. | — | — | Text Qualitative | main article p.976 · Results and Discussion · Figure S1 |
0.4 mg cm^-2 Ni3(HITP)2 GDE · Electrode
Catalyst layer scraped from AvCarb GDE after electrolysis; compared with AvCarb microporous layer background.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Ni3(HITP)2 crystallinity after GDE electrolysis | Ni3(HITP)2 retained crystallinity after polarization. | — | — | Text Qualitative | main article p.978 · Results and Discussion · Figures S10-S11 |