cMOF Evidence Base
Diffraction Structure — A Novel Electrocatalyst Pd(II)@Ni3(HITP)2 for Ultrasensitive Detection of Chloramphenicol: Experimental and Computational Investigation

Measurement evidence

Diffraction Structure

A Novel Electrocatalyst Pd(II)@Ni3(HITP)2 for Ultrasensitive Detection of Chloramphenicol: Experimental and Computational Investigation · He Y., Li N.-H., Wen F. et al. · Chemistry - A European Journal · 2023 · e202203839

1 measurement group · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR and powder XRD

Infrared spectroscopyX-ray diffraction and scattering

Pd(II)@Ni3(HITP)2, PdCl2 loading mass 0.05 mL/mg · Powder

FTIR spectra and XRD graph comparing Ni3(HITP)2 and Pd(II)@Ni3(HITP)2.

Geometry
powder comparison
Context
application_with_pristine_control
Measurement source
2-3 · Characterization and Loading Mechanism · Figure 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ar(C=C) FTIR band1626 cm-1 slight red shift after PdCl2 loading——Text
Rounded Reported		2 · Characterization and Loading Mechanism · Figure 1a
Pd(II)@Ni3(HITP)2 (200) peak shift0.8° to smaller angle——Text
Rounded Reported		2 · Characterization and Loading Mechanism · Figure 1b
Ni3(HITP)2 XRD assigned planes(100), (200), (001)——Text
Qualitative		2 · Characterization and Loading Mechanism · Figure 1b
PdCl2 (011) d-spacing in loaded MOFd(011)=2.53 Å——Text
Rounded Reported		3 · Characterization and Loading Mechanism · Figure 1b
pristine PdCl2 (011) d-spacing referenced(011)=2.51 Å——Text
Rounded Reported		3 · Characterization and Loading Mechanism · Figure 1b