Microscopy Morphology — A Novel Electrocatalyst Pd(II)@Ni3(HITP)2 for Ultrasensitive Detection of Chloramphenicol: Experimental and Computational Investigation

Measurement evidence

Microscopy Morphology

A Novel Electrocatalyst Pd(II)@Ni3(HITP)2 for Ultrasensitive Detection of Chloramphenicol: Experimental and Computational Investigation · He Y., Li N.-H., Wen F. et al. · Chemistry - A European Journal · 2023 · e202203839

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM elemental mapping

Pd(II)@Ni3(HITP)2, PdCl2 loading mass 0.05 mL/mg · Powder

Elemental maps for pristine and PdCl2-loaded samples at 0.02, 0.05, and 0.076 mL/mg.

Geometry
powder
Context
application_with_pristine_control
Measurement source
4 · Characterization and Loading Mechanism · Figures S5-S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM elemental distributionall elements distribute uniformlyText
Qualitative
4 · Characterization and Loading Mechanism · Figures S5-S8

SEM, TEM, HRTEM, SAED

Pd(II)@Ni3(HITP)2, PdCl2 loading mass 0.05 mL/mg · Powder

Morphology and lattice/fringe comparison before and after PdCl2 loading.

Geometry
powder
Context
application_with_pristine_control
Measurement source
4 · Characterization and Loading Mechanism · Figures 3-4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni3(HITP)2 HRTEM d(001)d(001)=0.661 nmVisual Estimate
Rounded Reported
4 · Characterization and Loading Mechanism · Figure 4b
PdCl2 HRTEM d(011)d(011)=0.248 nmVisual Estimate
Rounded Reported
4 · Characterization and Loading Mechanism · Figure 4e