Diffraction Structure — High-Performance H2S Sensors to Detect SF6 Leakage

Measurement evidence

Diffraction Structure

High-Performance H2S Sensors to Detect SF6 Leakage · Zhao X., Jiang S., Zhang Z. et al. · ACS Sensors · 2024 · 5512-5519

4 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

powder X-ray diffraction and Rietveld refinement after acid soaking

Co1.8Ni1.2(HITP)2 powder · Powder

Co1.8Ni1.2(HITP)2 soaked in pH 1 H2SO4 solution for 30 days.

Atmosphere
pH 1 H2SO4 solution
Context
chemical stability test of target mixed-metal powder
Measurement source
9 · Figure S3 · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
acid-soaking visual stabilitysolutions remain transparent without any color changesCaption
Qualitative
8 · Figure S2 · Figure S2
Rietveld Rp after pH 1 acid soakRp approximately 2.64%Visual Estimate
Rounded Reported
9 · Figure S3 · Figure S3
Rietveld Rwp after pH 1 acid soakRwp approximately 3.33%Visual Estimate
Rounded Reported
9 · Figure S3 · Figure S3

powder X-ray diffraction and Rietveld refinement after sensor stability testing

Co1.8Ni1.2(HITP)2 chemiresistive gas sensor on Au IDE chip · Electrode

Co1.8Ni1.2(HITP)2 scraped from sensor after 60 days of stability testing.

Geometry
scraped sensor material
Context
target device sample after sensing cycles
Measurement source
10 · Figure S4 · Figure S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Rietveld Rp after 60-day sensor stability testRp approximately 1.45%Visual Estimate
Rounded Reported
10 · Figure S4 · Figure S4
Rietveld Rwp after 60-day sensor stability testRwp approximately 1.84%Visual Estimate
Rounded Reported
10 · Figure S4 · Figure S4

powder X-ray diffraction and Rietveld refinement

Co1.8Ni1.2(HITP)2 powder · Powder

Fresh powder; Cu Kalpha radiation reported in SI.

Context
pristine mixed-metal powder
Measurement source
2 · Figure 1 caption · Figure 1a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Rietveld Rwp for fresh Co1.8Ni1.2(HITP)2Rwp = 1.68%Text
Exact Reported
2 · 2.1. Sample Preparation and Characterization · Figure 1a

powder X-ray diffraction

Co1.8Ni1.2(HITP)2 powder · Powder

XRD spectra for CoxNi3-x(HITP)2 compositions x = 0, 0.6, 1.2, 1.5, 1.8, 2.4 and 3.

Context
pristine family screening
Measurement source
7 · Figure S1 · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
XRD composition series coveredx = 0, 0.6, 1.2, 1.5, 1.8, 2.4, and 3Caption
Exact Reported
7 · Figure S1 · Figure S1