powder X-ray diffraction and Rietveld refinement after acid soaking
Co1.8Ni1.2(HITP)2 powder · Powder
Co1.8Ni1.2(HITP)2 soaked in pH 1 H2SO4 solution for 30 days.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| acid-soaking visual stability | solutions remain transparent without any color changes | — | — | Caption Qualitative | 8 · Figure S2 · Figure S2 |
| Rietveld Rp after pH 1 acid soak | Rp approximately 2.64% | — | — | Visual Estimate Rounded Reported | 9 · Figure S3 · Figure S3 |
| Rietveld Rwp after pH 1 acid soak | Rwp approximately 3.33% | — | — | Visual Estimate Rounded Reported | 9 · Figure S3 · Figure S3 |