Microscopy Morphology — A one-dimensional conductive metal-organic framework with extended π-d conjugated nanoribbon layers

Measurement evidence

Microscopy Morphology

A one-dimensional conductive metal-organic framework with extended π-d conjugated nanoribbon layers · Shang S., Du C., Liu Y. et al. · Nature Communications · 2022 · 7599

3 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

optical microscopy and SEM

DDA-Cu MOF crystals / bulk precipitate · Powder

needle-like bulk crystals

Measurement source
3 · Results - Synthesis and characterization · Fig. 2a,b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
maximum crystal length>100 umText
Approximate
3 · Results - Synthesis and characterization · Fig. 2a,b

SEM, AFM/HRAFM, TEM and GIWAXS

DDA-Cu MOF film · Thin Film

films grown 12-72 h; 25 nm film for GIWAXS

Measurement source
4 · Results - Synthesis and characterization · Fig. 3; Supplementary Figs. 12-15
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
film thickness after 12 h growth~8 nmText
Approximate
4 · Results - Synthesis and characterization · Supplementary Fig. 12
film thickness after 72 h growthnearly 245 nmText
Approximate
4 · Results - Synthesis and characterization · Supplementary Fig. 12
GIWAXS q values0.44, 0.81, 1.6, 1.9 A-1Text
Exact Reported
4 · Results - Synthesis and characterization · Fig. 3c,d
HRAFM parallel pattern width~1.2 nmText
Approximate
4 · Results - Synthesis and characterization · Fig. 3e; Supplementary Fig. 14

HRTEM

DDA-Cu MOF crystals / bulk precipitate · Powder

bulk lattice fringes

Measurement source
4 · Results - Synthesis and characterization · Fig. 2k,l; Supplementary Fig. 8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
HRTEM (001) lattice spacing~0.32 nmText
Approximate
4 · Results - Synthesis and characterization · Supplementary Fig. 8
HRTEM (100) lattice spacing~1.18 nmText
Approximate
4 · Results - Synthesis and characterization · Fig. 2l