Other — A one-dimensional conductive metal-organic framework with extended π-d conjugated nanoribbon layers

Measurement evidence

Other

A one-dimensional conductive metal-organic framework with extended π-d conjugated nanoribbon layers · Shang S., Du C., Liu Y. et al. · Nature Communications · 2022 · 7599

2 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

isolated yield

DDA-Cu MOF crystals / bulk precipitate · Powder

ethanol/water solution synthesis at 90 C for 24 h

Measurement source: 2 · Results - Synthesis and characterization · Fig. 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
isolated yield	85-92%	—	—	Text Range	2 · Results - Synthesis and characterization · Fig. 1

TGA and post-soak PXRD

X-ray diffraction and scattering Thermogravimetric analysis

DDA-Cu MOF crystals / bulk precipitate · Powder

TGA in N2; chemical soaking 24 h

Measurement source: 5 · Supplementary Figs. 9-10 · Supplementary Figs. 9-10

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
stability in 1 M HCl	crystallinity almost completely lost after 24 h	—	—	Qualitative Qualitative	5 · Supplementary Fig. 9 text · Supplementary Fig. 9
stability in neutral/basic media	PXRD intensity changed slightly after 24 h in boiling water, MeOH, DCM, THF, DMF and 1 M NaOH	—	—	Qualitative Qualitative	5 · Supplementary Fig. 9 text · Supplementary Fig. 9
initial decomposition temperature	approximately 320 C	—	—	Text Approximate	4 · Results - Synthesis and characterization · Supplementary Fig. 10