Microscopy Morphology — Enhancing Electrical Conductivity of Semiconducting MOFs via Defect Healing

Measurement evidence

Microscopy Morphology

Enhancing Electrical Conductivity of Semiconducting MOFs via Defect Healing · Choi J.Y., Park J. · ACS Applied Electronic Materials · 2021 · 4197-4202

4 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

HRTEM

HAB-treated Cu3(HAB)2, 30 min · Pellet

TEM at 300 kV; dose rate maintained between 20 and 50 e Angstrom^-2 s^-1.

Context
treated sample structure verification
Measurement source
3 · Results and Discussion · Figure 2d,e
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
d100 spacingd100 = 11.6 AngstromText
Exact Reported
3 · Results and Discussion · Figure 2d,e
hexagonal pore size~7 AngstromText
Approximate
3 · Results and Discussion · Figure 2d,e

Particle-size analysis; microscopy method not explicit in main-text sentence

HAB-treated Cu3(HAB)2, 30 min · Pellet

Average particle size compared before and after HAB treatment.

Context
treated versus pristine Cu3(HAB)2
Measurement source
3 · Results and Discussion
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
average particle size before HAB treatment29 nmText
Rounded Reported
3 · Results and Discussion
average particle size after HAB treatment31 nmText
Rounded Reported
3 · Results and Discussion

Scanning electron microscopy (SEM)

HAB-treated Co3(HAB)2 · Pellet

Particle size before and after post-treatment for Co3(HAB)2.

Context
treated analogue sample versus pristine analogue
Measurement source
5 · Results and Discussion · Figure S13 cited
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co3(HAB)2 particle size before treatment56 nmapproximatelyText
Approximate
5 · Results and Discussion · Figure S13 cited
Co3(HAB)2 particle size after treatment54 nmapproximatelyText
Approximate
5 · Results and Discussion · Figure S13 cited

Scanning electron microscopy (SEM)

TATHB-treated Cu3(TATHB)2 · Pellet

Particle size before and after post-treatment for Cu3(TATHB)2.

Context
treated analogue sample versus pristine analogue
Measurement source
5 · Results and Discussion · Figure S12 cited
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu3(TATHB)2 particle size before treatment66 nmapproximatelyText
Approximate
5 · Results and Discussion · Figure S12 cited
Cu3(TATHB)2 particle size after treatment68 nmapproximatelyText
Approximate
5 · Results and Discussion · Figure S12 cited