Microscopy Morphology — Superior Charge Transport in Ni-Diamine Conductive MOFs

4 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Pristine Cu3(HITT)2 black powder · Powder

Cryo-HRTEM at 200 kV; sonicated in isopropanol and drop-cast onto C-flat Cu grids.

Measurement source: 20502 · Results and discussion · Figure 2d,g; Figure S16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
large-pore/fringe periodicity	2.3 nm	—	—	Text Rounded Reported	20502 · Results and discussion · Figure 2g
pi-pi stacking spacing	0.33 nm	—	—	Text Rounded Reported	20502 · Results and discussion · Figures S16 and S17

Pristine Ni3(HITT)2 black powder · Powder

Cryo-HRTEM at 200 kV; sonicated in isopropanol and drop-cast onto C-flat Cu grids.

Measurement source: 20502 · Results and discussion · Figure 2e,g; Figure S17

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
large-pore/fringe periodicity	2.3 nm	—	—	Text Rounded Reported	20502 · Results and discussion · Figure 2g
pi-pi stacking spacing	0.33 nm	—	—	Text Rounded Reported	20502 · Results and discussion · Figures S16 and S17

Pristine Cu3(HITT)2 black powder · Powder

SEM at MIT MRSEC on Zeiss Merlin; operating voltage 1-4 kV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
morphology	well-defined nanorods	—	—	Text Qualitative	20502 · Results and discussion · Figure S15

Pristine Ni3(HITT)2 black powder · Powder

SEM at MIT MRSEC on Zeiss Merlin; operating voltage 1-4 kV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
particle size upper bound	100-200 nm	—	—	Text Range	20502 · Results and discussion · Figure S11
particle size lower bound	100-200 nm	—	—	Text Range	20502 · Results and discussion · Figure S11