Other — Chemical Vapor Deposition and High-Resolution Patterning of a Highly Conductive Two-Dimensional Coordination Polymer Film

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

RF-sputtered CuO precursor films · Thin Film

M-2000X or iSE Woollam instrument; optical modelling with CompleteEASE; CuO fitted using a B-spline model.

Geometry: thin-film precursor on substrate
Context: oxide precursor
Measurement source: SI p.S6 and p.S10 · Spectroscopic ellipsometry · Figure S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
CuO precursor thickness, Figure S5a	Thickness = 3.09 +/- 0.11 nm	—	+/- 0.11 nm	Figure Axis Rounded Reported	SI p.S10 · Results and Discussion · Figure S5a
CuO precursor thickness, Figure S5b	Thickness = 11.37 +/- 0.09 nm	—	+/- 0.09 nm	Figure Axis Rounded Reported	SI p.S10 · Results and Discussion · Figure S5b

H6BHT linker powder · Powder

Heating rate 5 deg C min^-1 under synthetic air or nitrogen flow.

Atmosphere: synthetic air or nitrogen
Context: molecular precursor, not framework
Measurement source: SI p.S5 and p.S8 · Thermogravimetric analysis · Figure S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
H6BHT stable at sublimation temperature range	stable at the sublimation temperature range	—	—	Caption Qualitative	SI p.S8 · Results and Discussion · Figure S2

H6BHT linker powder · Powder

Netzsch STA 449F3 Jupiter under dynamic vacuum 2 x 10^-3 mbar; isothermal steps every 10 deg C.

Atmosphere: dynamic vacuum
Geometry: alumina Knudsen effusion cell
Context: molecular precursor, not framework
Measurement source: SI p.S5 and p.S8 · Vapor pressure measurements · Figure S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
H6BHT vapour pressure threshold for CVD	>1 Pa at temperatures above 140 deg C	—	—	Text Approximate	main p.2 / article p.B · Results and Discussion · Figure 1d; Figure S1