Electrochemistry Application — From 0D to 2D: Microwave-assisted synthesis of electrically conductive metal-organic frameworks with controlled morphologies

7 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

0D Cu-HHTP/PTFE glassy-carbon electrode · Electrode

Three-electrode Biologic VSP-300 setup; Pt counter electrode; nonaqueous Ag/AgNO3 reference; scan rates for ECSA ranged 100-500 mV s-1.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
0D Cu-HHTP gravimetric capacitanceMarked as a best value within this paper	47.27 F g-1	—	—	Text Exact Reported	main p.3171 · Electrochemical characterization · Fig. 4b
CV redox feature common to all morphologies	-1.1 V vs. Ag/AgCl	—	—	Text Rounded Reported	main p.3171 · Electrochemical characterization · Fig. S14a
0D Cu-HHTP ECSAMarked as a best value within this paper	5.63 mF cm-2	—	—	Text Exact Reported	main p.3171 · Electrochemical characterization · Fig. 4b, Fig. S14b, Fig. S15

1D Cu-HHTP/PTFE glassy-carbon electrode · Electrode

Three-electrode Biologic VSP-300 setup; Pt counter electrode; nonaqueous Ag/AgNO3 reference; scan rates for ECSA ranged 100-500 mV s-1.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
1D Cu-HHTP gravimetric capacitance	about 23 F g-1 from Fig. 4b bar	—	visual estimate from bar/error plot	Visual Estimate Approximate	main p.3171 · Electrochemical characterization · Fig. 4b
1D Cu-HHTP ECSA	3.26 mF cm-2	—	—	Text Exact Reported	main p.3171 · Electrochemical characterization · Fig. 4b, Fig. S14b, Fig. S15

2D Cu-HHTP/PTFE glassy-carbon electrode · Electrode

Three-electrode Biologic VSP-300 setup; Pt counter electrode; nonaqueous Ag/AgNO3 reference; scan rates for ECSA ranged 100-500 mV s-1.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
2D Cu-HHTP gravimetric capacitance	about 24 F g-1 from Fig. 4b bar	—	visual estimate from bar/error plot	Visual Estimate Approximate	main p.3171 · Electrochemical characterization · Fig. 4b
2D Cu-HHTP ECSA	3.53 mF cm-2	—	—	Text Exact Reported	main p.3171 · Electrochemical characterization · Fig. 4b, Fig. S14b, Fig. S15

0D Cu-HHTP/PTFE glassy-carbon electrode · Electrode

Three-electrode Biologic VSP-300 setup using MOF/PTFE glassy-carbon electrodes.

Atmosphere: Electrolyte degassed with nitrogen.
Geometry: MOF/PTFE drop-cast glassy carbon working electrode.
Context: Electrode composite containing pristine Cu-HHTP active powder.
Measurement source: main p.3171 · Electrochemical characterization · Fig. 4c

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
0D Cu-HHTP EIS resistance trendMarked as a best value within this paper	0D shows less resistance than 1D and 2D	—	—	Text Qualitative	main p.3171 · Electrochemical characterization · Fig. 4c

0D Cu-HHTP/Nafion ITO photocurrent electrode · Electrode

0.5 M Na2SO4 electrolyte; MOF/Nafion slurry drop-cast on ITO glass; working electrode back-illuminated through ITO.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
0D Cu-HHTP transient photocurrent plateauMarked as a best value within this paper	about 1.3 mA cm-2 during illumination from Fig. 4d	—	visual estimate from plot	Visual Estimate Approximate	main p.3171 · Electrochemical characterization · Fig. 4d

1D Cu-HHTP/Nafion ITO photocurrent electrode · Electrode

0.5 M Na2SO4 electrolyte; MOF/Nafion slurry drop-cast on ITO glass; working electrode back-illuminated through ITO.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
1D Cu-HHTP transient photocurrent plateau	about 0.6 mA cm-2 during illumination from Fig. 4d	—	visual estimate from plot	Visual Estimate Approximate	main p.3171 · Electrochemical characterization · Fig. 4d

2D Cu-HHTP/Nafion ITO photocurrent electrode · Electrode

0.5 M Na2SO4 electrolyte; MOF/Nafion slurry drop-cast on ITO glass; working electrode back-illuminated through ITO.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
2D Cu-HHTP transient photocurrent plateau	about 0.5 mA cm-2 during illumination from Fig. 4d	—	visual estimate from plot	Visual Estimate Approximate	main p.3171 · Electrochemical characterization · Fig. 4d