Microscopy Morphology — From 0D to 2D: Microwave-assisted synthesis of electrically conductive metal-organic frameworks with controlled morphologies

6 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

0D spherical Cu-HHTP powder · Powder

EDS elemental analysis for Cu, C and O in 0D, 1D and 2D Cu-HHTP.

Geometry: Powder SEM-EDS.
Context: Pristine powders.
Measurement source: main p.3169 · Synthesis of Cu-HHTP with different morphologies · Fig. S8, Table S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
0D Cu-HHTP EDS carbon atomic percentage	77.23 At%	—	—	SI Table Exact Reported	SI p.S8 · Additional characterizations · Table S2
0D Cu-HHTP EDS copper atomic percentage	5.24 At%	—	—	SI Table Exact Reported	SI p.S8 · Additional characterizations · Table S2
0D Cu-HHTP EDS oxygen atomic percentage	17.53 At%	—	—	SI Table Exact Reported	SI p.S8 · Additional characterizations · Table S2

1D rod-like Cu-HHTP powder · Powder

EDS elemental analysis for Cu, C and O in 0D, 1D and 2D Cu-HHTP.

Geometry: Powder SEM-EDS.
Context: Pristine powders.
Measurement source: main p.3169 · Synthesis of Cu-HHTP with different morphologies · Fig. S8, Table S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
1D Cu-HHTP EDS copper atomic percentage	6.51 At%	—	—	SI Table Exact Reported	SI p.S8 · Additional characterizations · Table S2

2D sheet-like Cu-HHTP powder · Powder

EDS elemental analysis for Cu, C and O in 0D, 1D and 2D Cu-HHTP.

Geometry: Powder SEM-EDS.
Context: Pristine powders.
Measurement source: main p.3169 · Synthesis of Cu-HHTP with different morphologies · Fig. S8, Table S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
2D Cu-HHTP EDS copper atomic percentage	5.90 At%	—	—	SI Table Exact Reported	SI p.S8 · Additional characterizations · Table S2

0D spherical Cu-HHTP powder · Powder

SEM carried out on Hitachi SU3500; Fig. 2 contains SEM images and size distributions for 0D, 1D and 2D Cu-HHTP.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
0D Cu-HHTP sphere diameter after 15 min	ca. d = 3.55 um	—	ca.	Text Approximate	main p.3169 · Results and discussion · Fig. 2a
0D sphere diameter at 5 min growth	approximately 0.70 um at 5 min	—	approximately	Text Approximate	main p.3169 · Growth mechanism · Fig. 3

1D rod-like Cu-HHTP powder · Powder

SEM carried out on Hitachi SU3500; Fig. 2 contains SEM images and size distributions for 0D, 1D and 2D Cu-HHTP.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
1D Cu-HHTP rod diameter distribution centre	about 0.15-0.18 um from Fig. 2b histogram	—	visual estimate from histogram	Visual Estimate Approximate	main p.3170 · Results and discussion · Fig. 2b
1D Cu-HHTP rod length distribution centre	about 1.3-1.5 um from Fig. 2b histogram	—	visual estimate from histogram	Visual Estimate Approximate	main p.3170 · Results and discussion · Fig. 2b

2D sheet-like Cu-HHTP powder · Powder

SEM carried out on Hitachi SU3500; Fig. 2 contains SEM images and size distributions for 0D, 1D and 2D Cu-HHTP.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
2D Cu-HHTP sheet lateral length distribution centre	about 0.4-0.5 um from Fig. 2c histogram	—	visual estimate from histogram	Visual Estimate Approximate	main p.3170 · Results and discussion · Fig. 2c
2D Cu-HHTP sheet thickness distribution centre	about 0.10 um from Fig. 2c histogram	—	visual estimate from histogram	Visual Estimate Approximate	main p.3170 · Results and discussion · Fig. 2c